Preparation method of double sizing agent modified carbon fiber reinforced epoxy resin based composite
An epoxy resin, fiber reinforced technology, used in carbon fiber, fiber treatment, textiles and papermaking, etc., can solve the problems of increased defects, incomplete modification, unfavorable impact resistance, etc., to improve the interface shear performance, improve The effect of improving mechanical properties and tensile strength
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Embodiment 1
[0044] Amino multi-walled carbon nanotubes (CNTs) used in this example were purchased by Beijing Boyu Gaoke New Material Technology Co., Ltd., with a purity of 98%-99.999%; octaaminopropyl polyhedral oligomeric silsesquioxane (OA- POSS) is provided by the School of Chemical Engineering, Hebei University of Technology, with a purity of 97%-99.988%; tetraethyl orthosilicate (TEOS) concentration is more than 95%, ethanol (C 2 h 5 OH) concentration is 70%-90%, ammonia water (NH 3 OH) concentration is 70%-80%, and the above basic chemical materials are all pure substances for chemical analysis. The carbon fiber cloth is T300.
[0045] The steps of the preparation method of the double sizing agent modified carbon fiber reinforced epoxy resin-based composite material in this embodiment are:
[0046] 1) Preparation of carbon nanotube modified solution: dissolving silane coupling agent in ethanol solution, stirring at a speed of 1000r / min to obtain silane coupling agent sol; then si...
Embodiment 2
[0054]The steps for preparing the modified carbon fiber reinforced epoxy resin-based composite material in this example are the same as in Example 1, except that the mass percentage of each substance in the carbon nanotube modification solution described in this example is: 0.5% silane Joint agent sol, 1.0% amino multi-walled carbon nanotubes, 98.5% dispersant.
Embodiment 3
[0056] The steps of modifying the carbon fiber reinforced epoxy resin-based composite material in this example are the same as in Example 1, except that the mass percentage of each substance in the carbon nanotube modification solution described in this example is: 0.5% silane coupling Solvent sol, 2.0% amino multi-walled carbon nanotubes, 97.5% dispersant.
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