A kind of catalyst used for producing methyl ethyl ketone and preparation method thereof
A catalyst, methyl ethyl ketone technology, applied in the field of catalysts used in the production of methyl ethyl ketone and its preparation, to achieve the effects of good hydrothermal stability, wide application range, improved accessibility and physical transfer performance
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Embodiment 1
[0025] A kind of preparation method of the used catalyst of producing methyl ethyl ketone is realized by following steps:
[0026] 1) Preparation of carrier
[0027] First add sodium aluminate and water into the beaker and stir evenly, then add [choline][aspartic acid] ionic liquid and continue stirring
[0028] 1h; then add tetraethyl silicate dropwise and continue to stir for 2h, adjust the pH value to 10 with ammonia water to obtain a mixture; transfer the mixture to a polytetrafluoroethylene crystallization tank at 130°C for 72h, after After filtering and washing, dry at 105°C for 12h, and then roast at 550°C for 5h to obtain KIT molecular sieve; wherein, SiO in the mixture 2 、Al 2 o 3 , The molar ratio of [choline][aspartic acid] ionic liquid to deionized water is 1.0:0.05:0.02:120;
[0029] 2) Carrier pretreatment
[0030] Place the KIT molecular sieve in a 1mol / L ammonium nitrate solution for ion exchange. The operating conditions are stirring at 60°C for 15 hours,...
Embodiment 2
[0035] A kind of preparation method of catalyst used for producing methyl ethyl ketone is realized by following steps:
[0036] 1) Preparation of carrier
[0037] First add sodium aluminate and water into the beaker and stir evenly, then add [choline][aspartic acid] ionic liquid and continue stirring
[0038] 1h; then add tetraethyl silicate dropwise and continue to stir for 2h, adjust the pH value to 12 with ammonia water to obtain a mixture; transfer the mixture to a polytetrafluoroethylene crystallization tank at 160°C for 48h, after After filtering and washing, dry at 105°C for 12h, and then roast at 550°C for 5h to obtain KIT molecular sieve; wherein, SiO in the mixture 2 、Al 2 o 3 , The molar ratio of [choline][aspartic acid] ionic liquid to deionized water is 1.0:0.05:0.05:120;
[0039] 2) Carrier pretreatment
[0040] Place the KIT molecular sieve in 1mol / L ammonium nitrate solution for ion exchange. The operating conditions are stirring at 80°C for 12h, followed by...
Embodiment 3
[0045] A kind of preparation method of the used catalyst of producing methyl ethyl ketone is realized by following steps:
[0046] 1) Preparation of carrier
[0047] First add sodium aluminate and water into the beaker and stir evenly, then add [choline][aspartic acid] ionic liquid and continue stirring
[0048] 1h; then add tetraethyl silicate dropwise and continue stirring for 2h, adjust the pH value to 11 with ammonia water to obtain a mixture; transfer the mixture to a polytetrafluoroethylene crystallization tank at 145°C for 60h, after After filtering and washing, dry at 105°C for 12h, and then roast at 550°C for 5h to obtain KIT molecular sieve; wherein, SiO in the mixture 2 、Al 2 o 3 , The molar ratio of [choline][aspartic acid] ionic liquid to deionized water is 1.0:0.05:0.035:120;
[0049] 2) Carrier pretreatment
[0050] Place the KIT molecular sieve in 1mol / L ammonium nitrate solution for ion exchange. The operating conditions are stirring at 70°C for 13h, foll...
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