A kind of preparation method of u-mo-zr alloy
A u-mo-zr, alloy technology, applied in the field of U-Mo-Zr alloy preparation, can solve the problems of long process cycle, material loss and impurity increase, achieve high alloy purity, improve alloy uniformity, improve Effect of Alloy Purity
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Embodiment 1
[0054] Example 1 Preparation of U-8Mo-2Zr alloy
[0055] (1) U-8Mo alloy was prepared by one-time alloying in graphite crucible
[0056] The inner surface of the graphite crucible, the outer surface of the graphite sieve plate and the sieve holes are plasma-sprayed with calcium zirconate coating. Such as figure 1 As shown, the proportion of molybdenum raw material is adjusted to 8.3wt.%. Molybdenum wire is placed under the graphite sieve plate, uranium ingots are placed on the graphite sieve plate, the diameter of the graphite sieve plate is 5mm, and the center line of the adjacent sieve The distance between them is 10mm, the sieve holes are equidistantly distributed, and the thickness of the sieve plate is 8mm. After the raw materials are placed, the furnace is vacuumed to 5*10 -2 After Pa, the power is turned on. After the material is completely melted, it is kept at 1500°C for 30 minutes, and the temperature is lowered to 1200°C at a rate of 10°C / min. After that, the pow...
Embodiment 2
[0061] Example 2 Preparation of U-2Mo-8Zr alloy
[0062] (1) Prepare U-2Mo alloy by one-time alloying in graphite crucible
[0063] The inner surface of the graphite crucible, the outer surface of the graphite sieve plate and the sieve holes are plasma-sprayed with calcium zirconate coating. Such as figure 1 As shown, the proportion of molybdenum raw material is adjusted to 2.2wt.%. Molybdenum wire is placed under the graphite sieve plate, uranium ingots are placed on the graphite sieve plate, the diameter of the graphite sieve plate is 5mm, and the center line of the adjacent sieve The distance between them is 10mm, the sieve holes are equidistantly distributed, and the thickness of the sieve plate is 8mm. After the raw materials are placed, the furnace is vacuumed to 5*10 -2 After Pa, the power is turned on, and after the material is completely melted, it is kept at 1450°C for 25 minutes, and the temperature is lowered to 1200°C at a rate of 12°C / min.
[0064] (2) Using ...
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