Preparation method of high-adsorbability ion exchange resin for sewage treatment
An ion exchange resin, high adsorption technology, applied in water/sewage treatment, adsorption water/sewage treatment, water/sludge/sewage treatment, etc., can solve a large amount of sludge and other problems, and achieve strong water retention and selectivity High, high adsorption activity effect
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Embodiment 1
[0019] A method for preparing a highly adsorbent ion-exchange resin for sewage treatment, comprising the steps of:
[0020] S1. Swell the macroporous chloromethylated polystyrene resin into piperazine aqueous solution, add 2-aminoethanol, heat up, stir, cool down, wash, add modified guar gum and bamboo charcoal powder, stir evenly, filter, wash , drying to obtain pretreated polystyrene resin;
[0021] S2. In an ice-water bath, add thionyl chloride dropwise to the pretreated polystyrene resin, adjust the temperature, keep warm, cool down, wash, filter, send it to nitrobenzene for swelling, add trimethylamine to react, and obtain sewage treatment Highly absorbent ion exchange resin.
[0022] The modified guar gum is prepared by the following process: mix chitosan and glacial acetic acid evenly, add water and stir evenly, add polyethylene glycol, heat up and stir, heat up, add guar gum and stir to obtain the modified guar gum;
Embodiment 2
[0024] A method for preparing a highly adsorbent ion-exchange resin for sewage treatment, comprising the steps of:
[0025] S1. Send 60 parts by weight of macroporous chloromethylated polystyrene resin into 200 parts of 30 wt% piperazine aqueous solution for swelling for 8 hours, add 2 parts of 2-aminoethanol, heat up to 90°C, stir for 14 hours, and cool down , washing, adding 120 parts of modified guar gum, 5 parts of bamboo charcoal powder and stirring evenly, filtering, washing, and drying to obtain pretreated polystyrene resin;
[0026] S2. In an ice-water bath, add 4 parts of thionyl chloride dropwise to 100 parts of pretreated polystyrene resin by weight, adjust the temperature to 95°C, keep warm for 4 hours, cool down, wash, filter, and feed 280 parts of nitro Swell in benzene for 6 hours, add 13 parts of trimethylamine to react for 8 hours, and obtain high-adsorption ion-exchange resin for sewage treatment.
Embodiment 3
[0028] A method for preparing a highly adsorbent ion-exchange resin for sewage treatment, comprising the steps of:
[0029] S1. Send 70 parts by weight of macroporous chloromethylated polystyrene resin into 180 parts of 34 wt% piperazine aqueous solution to swell for 5 hours, add 4 parts of 2-aminoethanol, heat up to 70°C, stir for 20 hours, and cool down , washing, adding 100 parts of modified guar gum, 8 parts of bamboo charcoal powder and stirring evenly, filtering, washing, and drying to obtain pretreated polystyrene resin;
[0030] S2. In an ice-water bath, add 6 parts of thionyl chloride dropwise to 90 parts of pretreated polystyrene resin by weight, adjust the temperature to 85°C, keep warm for 8 hours, cool down, wash, filter, and feed 200 parts of nitro Swell in benzene for 10 hours, add 9 parts of trimethylamine and react for 12 hours to obtain a highly adsorbable ion exchange resin for sewage treatment.
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