Electrochromic cast resin laminated glass and method for the production thereof
A technology for casting resin and laminating glass, applied in synthetic resin layered products, lamination, lamination auxiliary operations, etc. The effect of improving the degree of cross-linking
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[0053] Example 1
[0054] The electrochromic laminated glass was prepared by gluing two ITO coated glasses made of 5mm float glass, which were connected along the edges by 1.5mm thick acrylic adhesive tape. Prepare 72g GmbH company UV (54g 2-ethylhexyl acrylate, 9g acrylic acid, 7.3g methyl methacrylate, 1.7g tris(2-methoxyethoxy) vinyl silane), 36g propylene carbonate, 36g poly(ethylene two Alcohol) diacrylate (M=700g / mol), 14.4g lithium trifluoromethanesulfonate, 0.2g 2,2-dimethoxy-2-phenylacetophenone and 1.6g ethylenedioxythiophene Mix the mixture and stir in the dark for 30 minutes. The mixture was filled into the cavity between two 300mm×300mm glass plates through a sleeve or funnel, and then the edge of the window was sealed with a two-component resin. Subsequently, one glass was cured in a UV radiation chamber for 30 minutes. By applying a DC voltage of 3.0V for 1 minute, a transparent polyethylenedioxythiophene film was formed on the anode, which turned blue when th...
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[0055] Example 2
[0056] The electrochromic laminated glass was prepared by gluing two ITO-coated glasses made of 5mm float glass, which were connected along the edges by 1.5mm thick acrylic adhesive tape. Prepare 25.6g methyl methacrylate, 22.4g 1,4-butanediol diacrylate, 3.2g pentaerythritol tetraacrylate, 6.4g 2-hydroxyethyl methacrylate, 6.4g methacrylic acid, 48g ethylene carbonate , 48g poly(ethylene glycol) diacrylate (M=700g / mol), 16g lithium perchlorate, 18.8g 3,4-(2,2-dimethylpropylenedioxy)thiophene (ProDOT- Me 2 ) And 0.28 g of 2,2-dimethoxy-2-phenylacetophenone, and stirred in the dark for 30 minutes. The mixture was filled into the cavity between two 300mm×300mm glass plates through a sleeve or funnel, and then the edge of the window was sealed with a two-component resin. Subsequently, the glass was cured in a UV radiation chamber for 30 minutes. By applying a DC voltage of 3.2V for 3 minutes, a transparent poly (proDOT-Me 2 ) Film, which turns blue-violet when ...
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