High-performance thermal barrier coating and ceramic layer thereof
A technology of thermal barrier coating and ceramic layer, applied in the direction of coating, metal material coating process, melt spraying, etc., can solve the problems of reducing the thermal cycle life of the coating, reducing the thermal insulation effect of the coating, etc., and achieving low cost , Improve efficiency and working temperature, the effect of simple process
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[0071] 1. Sol-spray pyrolysis synthesis powder.
[0072] With a purity of 99.99% Y (NO 3 ) 3 ·6H 2 O and Zr(NO 3 ) 4 ·3H 2 O is the raw material, in molar ratio Y(NO 3 ) 3 ·6H 2 O:Zr(NO 3 ) 4 ·3H 2 O=0.08:0.92 ingredients, using deionized water as a solvent, prepare an aqueous solution with a total concentration of metal ions of 0.2mol / L, stir magnetically for 1-3h until it is clear and transparent, then add additives such as citric acid hexahydrate and a molecular weight of 20000 Polyethylene glycol, wherein citric acid add-on 160g / L, polyethylene glycol 20g / L, stir until clear and transparent through magnetic force again, thereby make sol;
[0073] The above-prepared sol was atomized into a corundum crucible by a pressure atomization method, the atomization pressure was 0.3 MPa, and the temperature of the corundum crucible was 500°C. After the atomization of the sol, the temperature of the corundum crucible was raised to 1000°C for 2 hours and then cooled to room...
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