Plasticizing method for plant fiber raw materials
A plant fiber and fiber raw material technology, which is applied in the field of plant fiber raw material processing and application, can solve the problems of glycerin being difficult to solidify and high cost, and achieve the effect of low cost and simple and feasible process
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Embodiment 1
[0030] The method for plasticizing plant fiber raw materials with inorganic acid in this embodiment is carried out according to the following steps:
[0031] 1. Take 300g of dry wheat straw, and use a high-speed mixer to evenly disperse sulfuric acid in the middle of the wheat straw. The mass ratio of pure sulfuric acid to dry wheat straw is 5 / 100.
[0032] 2. Set the temperature of zones I, II, III, and IV of the twin-screw extruder to 160°C, 150°C, 130°C, and 120°C, respectively. Mixing the mixture obtained in step 1 in a twin-screw extruder with a set temperature to obtain a plasticized base material of wheat straw;
[0033] 3. Add the base material obtained in step 2 into the national standard abrasive tool, and use a flat vulcanizing machine to hot press at 160°C and a pressure of 20Mpa. A standard sample with a wheat straw content of 95wt% can be obtained. Its mechanical properties are shown in Table 1. The melting temperature of the base material is about 135°C when t...
Embodiment 2
[0037] 1. Take 300g of dry wheat straw, and use a high-speed mixer to evenly disperse sulfuric acid in the middle of the wheat straw. The ratio of the mass of pure sulfuric acid to the mass of dry wheat straw is 5 / 100.
[0038]2. Set the temperature of zones I, II, III, and IV of the twin-screw extruder to 160°C, 150°C, 130°C, and 120°C, respectively. The mixture obtained in step 1 is kneaded in a twin-screw extruder with a set temperature to obtain a plasticized base material of wheat straw.
[0039] 3. Mix 21.25g, 31.75g, 42.25g of maleic anhydride modified polyethylene with 75g, 65g, 55g of the plasticized material obtained in step 2, respectively, and set the temperature in zones I, II, III, and IV of the twin-screw extruder to The settings are 170°C, 150°C, 130°C, 120°C. The mixture is kneaded and extruded in a set twin-screw extruder to obtain a composite material of maleic anhydride polyethylene and wheat straw plasticized base material.
[0040] 4. Add the composite ...
Embodiment 3
[0044] 1. Take 300g of dry wheat straw, and use a high-speed mixer to evenly disperse sulfuric acid in the middle of the wheat straw. The ratio of the mass of pure sulfuric acid to the mass of dry wheat straw is 5 / 100.
[0045] 2. Set the temperature of zones I, II, III, and IV of the twin-screw extruder to 160°C, 150°C, 130°C, and 120°C, respectively. The mixture obtained in step 1 is kneaded in a twin-screw extruder with a set temperature to obtain the wheat straw plasticized base material.
[0046] 3. Mix 31.75g of maleic anhydride modified polyethylene with 65g of the plasticized base material obtained in step 2, and set the temperature in zones I, II, III, and IV of the twin-screw extruder to 170°C, 150°C, and 130°C respectively , 120°C. The mixture is kneaded and extruded in a set twin-screw extruder to obtain a composite material of maleic anhydride modified polyethylene and wheat straw plasticized base material.
[0047] 4. After crushing the above composite materi...
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