Alkali-free viscoelastic surfactant composition and its preparation method and application
A technology of surfactant and composition, applied in the field of preparation of alkali-free viscoelastic surfactant, can solve problems such as formation blockage and injection difficulty, and achieve the effects of reducing repulsion, high interfacial activity, and reducing critical micelle concentration
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Embodiment 1
[0031] 1. Surfactant Preparation
[0032] (1) Erucamide carboxy betaine surfactant (R 1 =C 21 , R 2 =C 3 , R 3 =C 2 ) preparation
[0033] a) Add 0.5 mole of methyl erucate and the required amount of amidating reagent N,N-dimethylpropylenediamine into the reaction kettle, react at 140°C for 8 hours, turn on the vacuum pump, and remove the methanol and Excess N,N-dimethylpropanediamine to obtain erucic acid acyl tertiary amide product, then add the required amount of sodium chloroacetate, react at 75°C for 9 hours, recrystallize and purify with absolute ethanol to obtain a long carbon chain Betaine surfactant; Wherein, methyl erucate: N, N-dimethylpropylenediamine: the mol ratio of sodium chloroacetate is 1:2.5:1.5.
[0034] b) Naphthalene sulfonate and the erucamide carboxy betaine surfactant prepared by the present invention were dissolved in water respectively, stirred for 30 minutes, and formulated into an aqueous solution, and then the above-mentioned surfactant was...
Embodiment 2
[0043] 1. Surfactant Preparation
[0044] (1) triacic acid amide carboxy betaine surfactant (R 1 =C 29 , R 2 =C 2 , R 3 =C 2 ) preparation
[0045] a) Add 0.5 mole of long-chain triacic acid methyl ester and the required amount of amidating reagent N,N-dimethylethylenediamine into the reaction kettle, react at 130°C for 6 hours, turn on the vacuum pump, and pump out the reaction Produced methanol and excess N,N-dimethylethylenediamine to obtain triacyl tertiary amine product, then add the required amount of sodium chloroacetate, react at 85°C for 15 hours, and recrystallize and purify with absolute ethanol Afterwards, a long carbon chain betaine surfactant is obtained; wherein, the molar ratio of triacic acid methyl ester:N,N-dimethylethylenediamine:sodium chloroacetate is 1:2:1.5.
[0046] b) Naphthalene sulfonate and the triacic acid amide carboxy betaine surfactant prepared by the present invention were dissolved in water respectively, stirred for 30 minutes, and for...
Embodiment 3
[0050] 1. Surfactant Preparation
[0051] (1) nonanoic acid amide carboxy betaine surfactant (R 1 =C 8 , R 2 =C 3 , R 3 =C 3 ) preparation
[0052] a) Add 0.5 mole of nonanoic acid methyl ester and the required amount of amidating reagent N,N-dimethylpropylenediamine into the reaction kettle, react at 135°C for 10 hours, turn on the vacuum pump, and remove the methanol and Excess N,N-dimethylpropanediamine to obtain nonanoic acid acyl tertiary amine product, then add the required amount of β-chloropropionate sodium, react at 75°C for 10 hours, and recrystallize and purify with absolute ethanol A long carbon chain betaine surfactant is obtained; wherein, the molar ratio of methyl nonanoate:N,N-dimethylpropylenediamine:β-sodium chloropropionate is 1:2:1.6.
[0053] b) Naphthalene sulfonate and the nonanoic acid amide carboxyl betaine surfactant prepared by the present invention were dissolved in water respectively, stirred for 30 minutes, and formulated into an aqueous so...
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