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Salt pan technology for separating ingredients by temperature differences

A technology of salt field and temperature difference, which is applied in the fields of bisulphate preparation, alkali metal sulphite/sulphite, inorganic chemistry, etc. It can solve the problems of not reaching the predicted value, difficult to recycle, and difficult to evaporate brine, etc. Achieve the effect of improving work efficiency

Inactive Publication Date: 2018-06-29
地矿集团格尔木盐湖资源开发有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Salt pan is an important place needed for salt production. At present, the sun-dried salt pan on the salt lake uses the existing simple salt pan: use sun-dried to make the target minerals in the brine of the salt lake change from unsaturated to saturated, then precipitate the target minerals, and recover the target minerals Utilization, from the point of view of the purity of the target minerals, the target mineral impurity content of the simple salt field drying is more difficult for subsequent processing. From the perspective of the salt field utilization season, the simple salt field only uses part of the Spring Festival, the whole summer, part of the autumn sun evaporation, and no winter Therefore, the efficiency of salt fields needs to be improved. In terms of the degree of brine drying, simple salt fields only perform simple primary sun drying, while in the middle and late stages of sun drying, it is more difficult for brine to evaporate naturally, and the goal of remaining in brine at this time Minerals, because the content has not yet reached the predicted value, it is difficult to be recycled

Method used

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  • Salt pan technology for separating ingredients by temperature differences
  • Salt pan technology for separating ingredients by temperature differences
  • Salt pan technology for separating ingredients by temperature differences

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0067] Example 1: Using a certain brine, the quality of brine is shown in the following table:

[0068] Table 2 Raw brine quality status table

[0069]

[0070] When the brine evaporates to the following extent, there is no evaporation phenomenon in the brine, and it is accompanied by other phenomena

[0071] Table 3 The simple solarization process can control the quality status of brine to the best point

[0072]

[0073] At this time, the brine has become solid at night and liquid at noon during the day, and by measuring the specific evaporation coefficient, it can be seen that the brine has no evaporation phenomenon, and the small-scale experiment of simulating a conventional simple salt field does not know how to operate: all operations are conventional simple salt fields Not achievable.

[0074] After using the temperature difference between morning and evening to separate bischofite, the brine will continue to be sun-dried, and finally the composition of higher-q...

example 2

[0085] Example 2: Opinions on the production of potassium mixed salt from sulfate-type brine

[0086] A certain salt lake belongs to sulfate-type brine, and the evaporation route is (rock salt—rock salt + epsomite——rock salt + epsom salt+carnallite—rock salt+carnallite+bischroite—— halite + bischofite).

[0087] In the development and utilization of the salt lake, it was found that due to the Epsom salt (MgSO 4 ·7H 2 O) content is relatively large, and the local rainfall is relatively large, it is difficult for the actual brine evaporation to enter the carnallite stage, and the development of this salt lake has always lagged behind the development of other salt lakes.

[0088] In the salt field test stage, we found that every night-morning, a lot of epsom salt crystallized on the salt field (rock ore identification), and in the morning-noon-afternoon stage, the epsom salt disappeared (redissolved into the brine), In this way, it is quite difficult for the brine to evaporate...

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Abstract

The invention relates to the technical field of salt lake chemical engineering of inorganic chemical industry, and discloses a salt pan technology for separating ingredients by temperature differences. The salt pan technology comprises a temperature difference salt pan and a storage pool, wherein a system water inlet is formed in one side of the temperature difference salt pan; a water dischargingopening is formed in one side, far away from the system water inlet, of the temperature difference salt pan; the water discharging opening is communicated with the storage pool; a pump pool is arranged inside the storage pool; a water pump communicating with the temperature difference salt pan is arranged inside the pump pool; a system water outlet is formed in one side of the storage pool. The salt pan technology for separating ingredients by temperature differences and application have the advantages that for a hot solution after solid separation, pure solids are separated out in the cooling process by adding a proper amount of fresh water; the solids can be favorably and further purified; pure solids are beneficial for preparation of other salts (such as preparation of potassium sulphate from high-quality picromerite, preparation of potassium chloride and magnesium metal from high-purity salt pan carnallite, and preparation of potassium sulphate from high-purity magnesium sulfate heptahydrate).

Description

technical field [0001] The invention relates to the technical field of salt lake chemical industry in inorganic chemical industry, in particular to a salt field technology for separating components by temperature difference. Background technique [0002] Salt refers to a class of compounds in which metal ions or ammonium ions (NH4+) are combined with acid ions or non-metal ions. Such as sodium chloride, calcium nitrate, ferrous sulfate and ammonium acetate, etc., such as calcium sulfate, copper chloride, sodium acetate, generally speaking, salt is the product of metathesis reaction, salt and salt react to form new salt and new salt, salt React with alkali to generate new salt and new base, salt and acid react to generate new salt and new acid, such as sulfuric acid and sodium hydroxide to generate sodium sulfate and water, sodium chloride and silver nitrate to generate silver chloride and sodium nitrate, etc. There are also other reactions that form salts, such as displacem...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01D3/06C01D5/00C01D5/12C01F5/30C01F5/40C01F11/24
CPCC01D3/06C01D5/00C01D5/12C01F5/30C01F5/40C01F11/24
Inventor 朱昌河张柏顺王录庆
Owner 地矿集团格尔木盐湖资源开发有限公司
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