Carbon nanotube paper and preparation method thereof
A carbon nanotube paper, carbon nanotube technology, applied in paper, papermaking, textiles and papermaking, etc., can solve the problems of reducing carbon nanotube paper properties, poor mechanical properties, increasing costs, etc., to improve flexibility and bendability. , high cleanliness, stable structure
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[0035] The present invention also provides a kind of preparation method of above-mentioned carbon nanotube paper, and this method comprises the steps:
[0036] Step 1, dispersion: put carbon nanotubes in an alcohol solvent for ultrasonic dispersion to obtain a carbon nanotube dispersion; place chemical fibers in an alcohol solvent for high-speed dispersion to obtain a chemical fiber dispersion;
[0037] Step 2, mixing: mixing the chemical fiber dispersion and the carbon nanotube dispersion, and stirring at a high speed to obtain a uniform mixture;
[0038] Step 3, filtering: the mixed solution prepared in step 2 is placed in a corresponding filter device to filter, and carbon nanotube wet paper with uniform thickness is formed on the filter membrane;
[0039] Step 4, baking: Put the carbon nanotube wet paper and the filter membrane into the oven to bake to remove the solvent;
[0040] Step 5, tableting: peel the dried carbon nanotube paper from the filter membrane, and use a ...
Embodiment 1
[0052] Place carbon nanotubes in isopropanol solvent, the ratio of the mass (mg) of carbon nanotubes to the volume (mL) of isopropanol solvent is 0.01mg / mL, and disperse in the isopropanol solvent by ultrasonic method Carbon nanotubes, ultrasonic power 60W, ultrasonic time 0.5h; dissolve polyethylene fibers in isopropanol solvent, disperse at 5000rpm for 1h, the ratio of the mass (mg) of chemical fibers to the volume (mL) of isopropanol solvent is 0.1 mg / mL; the molecular weight of polyethylene fiber is 3×10 4 , 70 nanometers in diameter, 350 microns in length; after the dispersion, the two dispersions were mixed and stirred at a high speed at 5000 rpm for 1 hour to obtain a uniform mixture; in the mixture, the mass ratio of carbon nanotubes to polyethylene fibers was 98:2; Transfer the uniform mixed solution into the filter device for vacuum filtration. The pumping rate of the vacuum pump is 1L / s, and the filter membrane is a polyethylene filter membrane; after the suction fi...
Embodiment 2
[0054] Place carbon nanotubes in ethanol and ethylene glycol solvent, the volume ratio (mL) of ethanol to ethylene glycol is 1:2, the ratio of the mass (mg) of carbon nanotubes to the volume (mL) of alcohol mixed solvent is 0.5mg / mL, use ultrasonic method to disperse carbon nanotubes in the alcohol mixed solvent, ultrasonic power 100W, ultrasonic time 0.5h; dissolve polypropylene fiber in ethanol solvent, disperse at 6000rpm for 1.5h, chemical fiber mass (mg) The ratio to the volume (mL) of ethanol solvent is 1mg / mL, in which polyethylene fiber, molecular weight 20×10 4 , with a diameter of 50 nanometers and a length of 300 microns; after the dispersion, mix the two dispersions and stir at a high speed of 8000rpm for 0.5h to obtain a uniform mixture; in the mixture, the mass ratio of carbon nanotubes to polypropylene fibers is 99.5:0.5 ;Transfer the uniform mixed solution into the filter device for pressure filtration, the pressure is 2MPa, and the filter membrane is a polytet...
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