Preparation method of wood and bamboo reinforced resin composites based on high pressure densification
A composite material and reinforced resin technology, applied in wood impregnation, wood treatment, impregnated wood, etc., can solve the problem of low added value of products
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[0040] The present invention is based on high-pressure compacted wood and bamboo reinforced resin composite material and preparation method thereof, comprising the following specific steps:
[0041] (1) Partial lignin and hemicellulose removal process: the starting raw material is wood veneer or waste board or bamboo sheet, using professional chemical reagents to remove part of lignin and hemicellulose in wood or bamboo, and washing with water Remove chemicals from lignin and hemicellulose wood or bamboo, and then use ethanol or acetone to replace the water in wood or bamboo;
[0042] The veneer is a wood board cut radially, chordwise or transversely from the wood, and the wood species is not particularly limited. The waste board is any discarded wood board, plywood, etc., without special limitation. The bamboo sheet is a sheet cut from bamboo, and the bamboo species include green bamboo, moso bamboo, and Ci bamboo. The thickness of the veneer, waste board, and bamboo sheet i...
Embodiment 1
[0063] Put poplar veneer (100mm×100mm×1mm) into NaOH (2.0mol / L) and NaOH at 80°C 2 SO 3 (0.5mol / L) mixed solution soaked for 2h, remove part of the lignin and hemicellulose in the veneer (removal rate is 50%), then use deionized water to repeatedly clean the veneer many times, remove excess chemical The substance was cleaned, and 5 similar veneers were prepared repeatedly, and then put into absolute ethanol, soaked for 30 minutes, and the water in the veneers was replaced. Flame retardant 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) and octaphenyl cage silsesquioxane (both additions are respectively 1% of resin weight) 5wt.%, 10wt.% in total), curing agent diphenyl sulfone (addition amount is 25wt.% of resin weight) added to E51 epoxy resin, stirred evenly, and then put the veneer into the resin mixing system, through vacuum impregnation The method is to infiltrate the resin into the veneer. Under vacuum conditions, the pressure in the vacuum tank is -0.02MPa, a...
Embodiment 2
[0065] Put poplar veneer (100mm×100mm×1mm) into NaOH (2.0mol / L) and NaOH at 80°C 2 SO 3 (0.5mol / L) mixed solution soaked for 2h, remove part of the lignin and hemicellulose in the veneer (removal rate is 40%), then use deionized water to repeatedly wash the veneer many times, remove excess chemical Clean the substance, then put it into acetone, soak for 30min, and replace the moisture in the wood; repeat the preparation of 4 similar veneers, and dry them naturally; then put them into a phenolic resin solution with a solid content of 25wt.%. Immerse in water for 10 minutes, take out the veneer, and let it dry naturally. Then put the veneer into an aqueous solution containing ammonium polyphosphate flame retardant (dimethyl methyl phosphate, the concentration of the flame retardant is 10wt.%) and soak for about 25min, so that the weight gain of the veneer reaches 10% (the weight gain of the flame retardant ), take out the veneer and let it dry again. Then five pieces of venee...
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