Preparation method of microcapsules with ovalbumin-inulin as wall material
A technology of ovalbumin and microcapsules, which is applied in the field of microcapsule preparation, can solve the problems of failure to achieve sustained release effect, damage to embedded materials, poor stability, etc., and achieve both health care effects, beneficial digestion and absorption, and sustained release effects Good results
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[0027] Preparation of oily core material:
[0028] Microcapsule core material preparation: prepare 15% (w / v) glutathione aqueous solution, join in the triglyceride of same quality, add 3% (w / w) soybean lecithin as emulsifier, under 12000r / min Disperse at a high speed for 4 minutes to prepare a W / O emulsion, and obtain the glutathione microcapsule core material as the oily core material in the following examples.
Embodiment 1
[0029] Embodiment 1 A method for preparing a novel microcapsule wall material using ovalbumin and inulin as the wall material, the specific steps are as follows:
[0030] (1) dissolving ovalbumin in water, and obtaining an ovalbumin dispersion after magnetic stirring, so that the ratio of ovalbumin is 1.0% w / w;
[0031] (2) Add inulin to the ovalbumin dispersion, the amount of inulin added is 1.0% w / w, the magnetic stirring frequency is 30rpm / min, and the ultrasonic intensity is 180W / cm 2 , sonication time is 1 hour. ;
[0032] (4) adding the oily core material into the ovalbumin-inulin solution in an amount of 5% w / w to obtain a mixed solution;
[0033] (5) The mixed solution of ovalbumin-inulin and oily core material is placed under a high-speed shearing apparatus and sheared for 1 min to obtain colostrum at a speed of 20,000 rpm / min. Quality three times.
[0034] (6) Spray-dry the ovalbumin-inulin and triglyceride mixed emulsion at an air inlet temperature of 170°C, an ...
Embodiment 2
[0036] Embodiment 2 A method for preparing a novel microcapsule wall material using ovalbumin and inulin as the wall material, the specific steps are as follows:
[0037] (1) dissolving ovalbumin in water, and obtaining an ovalbumin dispersion after magnetic stirring, so that the ratio of ovalbumin is 1.2% w / w;
[0038] (2) Add inulin to the ovalbumin dispersion, the amount of inulin added is 1.2% w / w, the magnetic stirring frequency is 40rpm / min, and the ultrasonic intensity is 200W / cm 2 , Ultrasonic time is 2 hours. ;
[0039] (4) adding the oily core material into the ovalbumin-inulin solution in an amount of 10% w / w to obtain a mixed solution;
[0040] (5) Place the mixed solution of ovalbumin-inulin and oily core material under a high-speed shearer and shear it for 1.5min to obtain colostrum at a speed of 25000rpm / min, and then circulate it under a pressure of 12kPa under high-pressure micro-jet Homogenize three times.
[0041] (6) Spray-dry the ovalbumin-inulin and tri...
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