Corrosion-resistant all-solid electrode for detecting marine electric field and preparation method thereof
An anti-corrosion, all-solid-state technology, applied in electrostatic field measurement, measuring devices, and measuring electrical variables, etc., can solve problems such as poor pressure and various stress tolerance, weak anti-interference ability of ions, and low mechanical strength of electrodes. Achieve the effect of improving corrosion resistance, large ion abundance, and avoiding weak combination
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Embodiment 1
[0024] Such as figure 1 As shown, the anti-corrosion all-solid-state electrode for marine electric field detection of the present invention has a structure including an electrode body, a sealing ring 5 and a copper pillar 6 . The main body of the electrode is made of silver wire 1 as the base material, which is covered with AgCl coating 2, quaternized chloromethyl polystyrene coating 3 and sulfonated polyaryletherketone-Nafion composite film 4 sequentially from the inside to the outside.
[0025] The electrode preparation method is as follows:
[0026] 1) AgCl coating: After polishing a section of silver wire with sandpaper, ultrasonically clean it in acetone and ultrapure water for 10 minutes, then immerse it in 0.1 M hydrochloric acid solution, and use constant current method at a current density of 0.5 mA / cm 2 Under the conditions of the reaction for two hours, a layer of dense AgCl coating grows on the surface of the silver wire;
[0027] 2) Quaternized chloromethyl poly...
Embodiment 2
[0031] The electrode of the present invention and the common Ag / AgCl electrode were put into simulated seawater to test their corrosion resistance. In order to make the experimental phenomenon more obvious, the Br in seawater will be simulated - The content was increased from 0.008 mol / L to 0.03 mol / L to speed up the corrosion rate. At the same time, the point changes of the two electrodes relative to the standard calomel reference electrode were tested. The experimental results are as follows figure 2 .
[0032] It can be known from the experiment that the Ag / AgCl electrode without anti-corrosion coating treatment is in the Br - After soaking in the rich simulated seawater for about 80 minutes, the potential began to decrease rapidly, which was mainly due to the Br - Cl in the double layer - The competition caused by fouling the AgCl coating at the same time, and the response of the corroded electrode to the electric field is greatly weakened. In contrast, the potential ...
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