High-temperature-resisting water-based well-drilling fluid filtrate reducer and preparation method thereof
A technology of water-based drilling fluid and fluid loss control agent, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of increased liquid phase viscosity of the system, unfavorable market competition, high cost of multi-component copolymers, etc., and achieve reduction The effect of high temperature and high pressure filtration loss, good high temperature resistance and filtration loss reduction ability, and good performance
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[0027] In the second aspect, the present invention also provides a method for preparing the high-temperature resistant water-based fluid loss additive for drilling fluid, which includes the following steps:
[0028] (1) After mixing the sulfomethyl phenolic resin with formaldehyde, adjust the pH of the solution to 8.0-8.5, and then add melamine to react to obtain a modified sulfomethyl phenolic resin;
[0029] (2) Stir the modified sulfomethyl phenolic resin, sulfonate monomers, acrylamide monomers, N,N-methylene bisacrylamide, and initiators, and then heat up to 30-50℃ Reaction to obtain a gel-like product;
[0030] (3) After granulating, drying and pulverizing the obtained gel-like product, the high-temperature resistant water-based fluid loss additive for drilling fluid is obtained.
[0031] The method of the present invention modifies the sulfomethyl phenolic resin and then copolymerizes with a variety of monomers, namely by increasing the hydration group of the product, introduci...
Embodiment 1
[0038] A high-temperature resistant water-based fluid loss additive for drilling fluid is prepared from the following parts by mass of raw materials: 700 parts of sulfomethyl phenolic resin, 3 parts of formaldehyde, 6 parts of melamine, 8 parts of sodium styrene sulfonate, 40 parts of acrylamide, 1 part of N,N-methylenebisacrylamide, 0.3 parts of oxygen reduction initiator (0.15 parts of ammonium persulfate, 0.15 parts of sodium bisulfite), and 60 parts of water.
[0039] First prepare sulfomethyl phenolic resin: add 50 parts of water, 160 parts of formaldehyde, 100 parts of phenol, 35 parts of sodium metabisulfite and 42 parts of sodium sulfite into the reaction kettle, react at 60°C for 45 minutes, then raise the temperature to 97°C, and pass batches Add 335 parts of water (including the first 50 parts, divide the water into 5 batches, each batch add 57 parts), observe the change of the viscosity of the reaction system, when the viscosity of the reaction product increases to a c...
Embodiment 2
[0045] A kind of anti-high temperature water-based drilling fluid fluid loss agent is prepared from the following parts by mass of raw materials: 700 parts of sulfomethyl phenolic resin, 3 parts of formaldehyde, 6 parts of melamine, 8 parts of sodium styrene sulfonate, N,N-2 40 parts of methacrylamide, 0.5 parts of N,N-methylenebisacrylamide, 0.3 parts of oxygen reduction initiator (0.15 parts of ammonium persulfate, 0.15 parts of sodium bisulfite), 70 parts of water.
[0046] First, prepare sulfomethyl phenolic resin: add 50 parts of water, 156.5 parts of formaldehyde, 100 parts of phenol, 37.25 parts of sodium metabisulfite and 35.5 parts of sodium sulfite into the reaction kettle, react at 60°C for 45 minutes, then increase the temperature to 97°C, and pass batches Add 335 parts of water (including the first 50 parts, divide the water into 5 batches, each batch add 57 parts), observe the change of the viscosity of the reaction system, when the viscosity of the reaction product ...
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