High-temperature-resisting water-based well-drilling fluid filtrate reducer and preparation method thereof

A technology of water-based drilling fluid and fluid loss control agent, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of increased liquid phase viscosity of the system, unfavorable market competition, high cost of multi-component copolymers, etc., and achieve reduction The effect of high temperature and high pressure filtration loss, good high temperature resistance and filtration loss reduction ability, and good performance

Inactive Publication Date: 2019-02-12
中科宝辰(北京)科技有限公司
View PDF10 Cites 3 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, if only high-temperature polymer fluid loss additives are used, it must be achieved by increasing the amount of polymer added. However, with the increase in the amount of polymer added, the viscosity of the liquid phase of the system will increase, which will bring new challenges to the rheological control of high-density drilling fluid. On the other hand, the cost of multi-component copolymers is generally much higher than that of high-temperature fluid loss additives currently on the market, which is not conducive to market competition

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • High-temperature-resisting water-based well-drilling fluid filtrate reducer and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0027] In the second aspect, the present invention also provides a method for preparing the high-temperature resistant water-based fluid loss additive for drilling fluid, which includes the following steps:

[0028] (1) After mixing the sulfomethyl phenolic resin with formaldehyde, adjust the pH of the solution to 8.0-8.5, and then add melamine to react to obtain a modified sulfomethyl phenolic resin;

[0029] (2) Stir the modified sulfomethyl phenolic resin, sulfonate monomers, acrylamide monomers, N,N-methylene bisacrylamide, and initiators, and then heat up to 30-50℃ Reaction to obtain a gel-like product;

[0030] (3) After granulating, drying and pulverizing the obtained gel-like product, the high-temperature resistant water-based fluid loss additive for drilling fluid is obtained.

[0031] The method of the present invention modifies the sulfomethyl phenolic resin and then copolymerizes with a variety of monomers, namely by increasing the hydration group of the product, introduci...

Embodiment 1

[0038] A high-temperature resistant water-based fluid loss additive for drilling fluid is prepared from the following parts by mass of raw materials: 700 parts of sulfomethyl phenolic resin, 3 parts of formaldehyde, 6 parts of melamine, 8 parts of sodium styrene sulfonate, 40 parts of acrylamide, 1 part of N,N-methylenebisacrylamide, 0.3 parts of oxygen reduction initiator (0.15 parts of ammonium persulfate, 0.15 parts of sodium bisulfite), and 60 parts of water.

[0039] First prepare sulfomethyl phenolic resin: add 50 parts of water, 160 parts of formaldehyde, 100 parts of phenol, 35 parts of sodium metabisulfite and 42 parts of sodium sulfite into the reaction kettle, react at 60°C for 45 minutes, then raise the temperature to 97°C, and pass batches Add 335 parts of water (including the first 50 parts, divide the water into 5 batches, each batch add 57 parts), observe the change of the viscosity of the reaction system, when the viscosity of the reaction product increases to a c...

Embodiment 2

[0045] A kind of anti-high temperature water-based drilling fluid fluid loss agent is prepared from the following parts by mass of raw materials: 700 parts of sulfomethyl phenolic resin, 3 parts of formaldehyde, 6 parts of melamine, 8 parts of sodium styrene sulfonate, N,N-2 40 parts of methacrylamide, 0.5 parts of N,N-methylenebisacrylamide, 0.3 parts of oxygen reduction initiator (0.15 parts of ammonium persulfate, 0.15 parts of sodium bisulfite), 70 parts of water.

[0046] First, prepare sulfomethyl phenolic resin: add 50 parts of water, 156.5 parts of formaldehyde, 100 parts of phenol, 37.25 parts of sodium metabisulfite and 35.5 parts of sodium sulfite into the reaction kettle, react at 60°C for 45 minutes, then increase the temperature to 97°C, and pass batches Add 335 parts of water (including the first 50 parts, divide the water into 5 batches, each batch add 57 parts), observe the change of the viscosity of the reaction system, when the viscosity of the reaction product ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
filtrationaaaaaaaaaa
Login to view more

Abstract

The invention discloses a high-temperature-resisting water-based well-drilling fluid filtrate reducer and a preparation method thereof. The high-temperature-resisting water-based well-drilling fluid filtrate reducer is prepared from the following raw materials in parts by mass: 700 parts of sulfomethylated phenol formaldehyde resin, 3-8 parts of formaldehyde, 6-15 parts of melamine, 8-20 parts ofa sulfonate monomer, 40-80 parts of an acrylamide monomer, 0.5-2 parts of a cross-linking agent, 0.3-0.6 part of an initiator, and 60-80 parts of water. The sulfomethylated phenol formaldehyde resin is modified and then subjected to a copolymerization with the multiple monomers, namely the high-temperature-resisting water-based well-drilling fluid filtrate reducer is synthesized by increasing hydration groups of a product and introducing new sulfonic groups and aromatic ring structures, thus the demand of safe well-drilling construction in a downhole high-temperature environment can be met, the rheological property and suspension stability of water-based well-drilling fluid under the high-temperature and high-pressure conditions can be controlled, and the high-temperature and high-pressurefilter loss of the well-drilling fluid is effectively decreased.

Description

Technical field [0001] The invention relates to a high-temperature resistant drilling fluid fluid loss agent and a preparation method thereof, and belongs to the technical field of oil field chemical preparation. Background technique [0002] As deep-seated oil and gas exploration and development efforts increase, the drilling encounters have become more and more complex. Generally speaking, the deeper the well, the higher the downhole pressure and temperature, and the greater the difficulty of drilling and completion. There are high temperature and high pressure formations in many parts of the world. In developed areas such as the United States and the North Sea, many reservoirs have pressures exceeding 100 MPa and bottom hole temperatures exceeding 200 ℃. In our country’s southwestern Tarim, Sichuan’s northeast of Sichuan, Daqing’s Xujiaweizi, and the ocean’s South China Sea Yingqiong Basin, there are different degrees of high temperature and high pressure drilling and comple...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/035C08F283/00C08F220/56C08F212/14
CPCC08F283/002C09K8/035C08F220/56C08F212/14
Inventor 黄伟
Owner 中科宝辰(北京)科技有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products