Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

A drying device for electrospray ionization coupled with ultrasonic atomization and method for preparing microcapsules

A technology of electrospray ionization and drying device, which is used in microcapsule preparation, spray evaporation, microsphere preparation and other directions to achieve the effect of reducing production energy consumption, reducing addition amount, and reducing size

Active Publication Date: 2021-02-19
JIANGSU UNIV +1
View PDF20 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this method does not break away from the limitations of the spray-drying method to prepare microcapsules, and still retains most of the defects of the spray-drying method.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A drying device for electrospray ionization coupled with ultrasonic atomization and method for preparing microcapsules
  • A drying device for electrospray ionization coupled with ultrasonic atomization and method for preparing microcapsules

Examples

Experimental program
Comparison scheme
Effect test

example 2

[0048] Example 2, the method for preparing vitamin C microcapsules by electrospray ionization coupling ultrasonic atomization

[0049] Prepare 500mL, 5% mass fraction of vitamin C aqueous solution and 2000mL, 0.2% mass fraction of sodium alginate aqueous solution respectively. 0.5% ethanol was added to the aqueous solution of sodium alginate to improve the atomization efficiency. Then slowly add 1M HCL / NaOH respectively to adjust the pH of the core material and wall material solutions to 7.0±0.2. After fully dissolving and mixing at room temperature (25±3°C), put the sodium alginate aqueous solution into the wall material liquid container 1, and put the vitamin C aqueous solution into the core material liquid container 9. All the sample solutions configured above should be used up on the same day, and the remaining samples can be temporarily stored at 4°C for 1-5 days after adding 0.05% NaCN by mass fraction.

[0050] When preparing the microcapsules, turn on the wall materi...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a drying machine adopting electrospray ionization coupling ultrasonic atomization and a method thereof used for preparing microcapsules. Wall material liquid is conveyed into an ultrasonic atomization container, the wall material liquid is atomized by an ultrasonic atomizer in the ultrasonic atomization container to form wall material droplets, and the wall material droplets enter a gas mixer; meanwhile, electrospray ionization is performed on a core material to form core material droplets, the core material droplets form charged particles through hot nitrogen, and thecharged particles enter the gas mixer through holes of a negative high-voltage electrode plate; a wall material and the core material are embedded in a spray drying bin, air passes through a filter and then is heated by a heater, the heated air is conveyed into the spray drying bin, the embedded particles are dried by the hot air, all grades of particles are separated by a gas-solid separator, themicrocapsules and macromolecule particles are collected by a collector, nanocapsules and micromolecule particles are collected by a dehumidifier and a particle collector, so that the energy-conversion, green and high-quality microcapsules with efficient instable nutrients are prepared under the synergism of electrospray ionization, ultrasonic atomization and spray drying.

Description

technical field [0001] The invention belongs to the technical field of microcapsule preparation, and in particular relates to a drying device for electrospray ionization coupled with ultrasonic atomization and a method for preparing microcapsules. Background technique [0002] Nutrients and related products currently on the market are mainly ingested orally, and have defects such as short storage time, low bioavailability, poor stability in the gastrointestinal tract, and easy degradation. The preparation of microcapsules by spray drying method is one of the main means to solve this problem. Compared with other embedding methods, it has the advantages of low operating cost, high production capacity, and simple process, but it also has low encapsulation efficiency and capsule particle size. Large diameter, poor product uniformity and other defects. Therefore, it is imperative to invent and create new microcapsule embedding technology. In recent years, electrospray ionizatio...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): B01J13/04B01D1/20B01D1/18B01D1/30
CPCB01D1/18B01D1/20B01D1/30B01J13/04B01J13/043
Inventor 王博王玉川魏本喜徐保国
Owner JIANGSU UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products