Preparation method of pressure-resistant oil filter paper
A technology of oil filter paper and pressure resistance, which is applied in the field of preparation of pressure-resistant oil filter paper, which can solve the problems of low pressure resistance and easy damage of filter paper, and achieve the effects of improving filtration accuracy, improving adsorption effect, and good adsorption function
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Embodiment 1
[0028] The preparation method of modified activated clay comprises the following steps:
[0029] Add the montmorillonite powder into a hydrochloric acid solution with a concentration of 3.5wt% and soak for 8 hours, the mass ratio of the montmorillonite and hydrochloric acid is 1:0.3, filter and separate, and dry at 60° C. for 2 hours to obtain the activated montmorillonite powder; Dodecyl dimethyl ammonium chloride is added in water and is mixed with concentration and is 15wt% glycidyl dodecyl dimethyl ammonium chloride aqueous solution, to epoxypropyl dodecyl dimethyl ammonium chloride aqueous solution Add alginic acid to the mixture, the mass ratio of epoxypropyl dodecyl dimethyl ammonium chloride to alginic acid is 1:8, react at 43°C for 25min, then add acetone, precipitate, wash and dry to obtain quaternary Ammonification modified alginic acid; adding activated montmorillonite powder into 4wt% calcium hydroxide water solution, wherein the mass ratio of activated montmorill...
Embodiment 2
[0036] The preparation method of modified activated clay comprises the following steps:
[0037] Add the montmorillonite powder into a 2.5wt% hydrochloric acid solution and soak for 6 hours, the mass ratio of the montmorillonite to hydrochloric acid is 1:0.3, filter and separate, and dry at 45° C. for 1.5 hours to obtain the activated montmorillonite powder; Glycidyl dodecyl dimethyl ammonium chloride is added in water and is mixed with concentration and is 12wt% glycidyl dodecyl dimethyl ammonium chloride aqueous solution, to epoxy propyl dodecyl dimethyl ammonium chloride Add alginic acid to the aqueous solution, the mass ratio of epoxypropyl dodecyl dimethyl ammonium chloride to alginic acid is 1:6, react at 41°C for 22 minutes, then add acetone, precipitate, wash and dry to obtain Quaternized modified alginic acid; adding activated montmorillonite powder into a water solution with a mass concentration of 2.5wt% calcium hydroxide, wherein the mass ratio of activated montmor...
Embodiment 3
[0044] The preparation method of modified activated clay comprises the following steps:
[0045] Add the montmorillonite powder into a 4.5wt% hydrochloric acid solution and soak for 8 hours, the mass ratio of the montmorillonite to hydrochloric acid is 1:0.4, filter and separate, and dry at 75° C. for 2.5 hours to obtain the activated montmorillonite powder; Glycidyl dodecyl dimethyl ammonium chloride is added in water and is mixed with concentration and is 18wt% glycidyl dodecyl dimethyl ammonium chloride aqueous solution, to epoxy propyl dodecyl dimethyl ammonium chloride Add alginic acid to the aqueous solution, the mass ratio of epoxypropyl dodecyl dimethyl ammonium chloride to alginic acid is 1:9, react at 44°C for 27 minutes, then add acetone, precipitate, wash and dry to obtain Quaternized modified alginic acid; add the activated montmorillonite powder into the calcium hydroxide solution with a mass concentration of 5wt%, wherein the mass ratio of the activated montmori...
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