Pretreatment method of conductive polyester fibers, conductive polyester fibers and preparation method thereof

A polyester fiber pretreatment technology, applied in fiber treatment, fiber type, wear-resistant fiber, etc., can solve the problems of fiber damage, fiber performance degradation, environmental pollution, etc., and achieve the effect of overcoming fiber damage and improving binding force

Inactive Publication Date: 2019-03-29
GUANGDONG UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The invention provides a pretreatment method of conductive polyester fiber, conductive polyester fiber and its preparation method, which solves the problems that the existing pretreatment of conductive polyester fiber will cause fiber damage, lead to deterioration of fiber performance, and easily cause environmental pollution

Method used

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  • Pretreatment method of conductive polyester fibers, conductive polyester fibers and preparation method thereof
  • Pretreatment method of conductive polyester fibers, conductive polyester fibers and preparation method thereof
  • Pretreatment method of conductive polyester fibers, conductive polyester fibers and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0048] (1) Pre-soak the polyester thread with a 5 g / L tannic acid solution at room temperature for 1 hour, take out the polyester thread, wash it with deionized water three times, and dry it to obtain a tannic acid-modified polyester thread.

[0049] (2) Soak the tannic acid-modified polyester thread in 50 g / L copper sulfate pentahydrate solution for 1 hour, take it out, and obtain the modified polyester thread that absorbs copper ions.

[0050] (3) Treat the modified polyester thread adsorbed with copper ions with 0.01 mol / L sodium borohydride for 180 s to obtain a polyester thread uniformly attached to the metallic copper activation catalyst layer.

[0051] (4) Dissolve 2.0g copper sulfate pentahydrate, 0.4g nickel sulfate hexahydrate, and 10.0g potassium sodium tartrate tetrahydrate in deionized water, then adjust the pH value of the solution with sodium hydroxide to obtain 500ml of dark blue with a pH value of 12 Solution: Take 2ml of 38% formaldehyde solution with a pipet...

Embodiment 2

[0055] (1) Pre-soak the polyester thread with a 10 g / L tannic acid solution at room temperature for 40 minutes, take out the polyester thread, wash it with deionized water three times, and dry it to obtain a tannic acid-modified polyester thread.

[0056] (2) Soak the tannic acid-modified polyester thread in 100 g / L copper sulfate pentahydrate solution for 2 hours, take it out, and obtain the modified polyester thread that absorbs copper ions.

[0057] (3) The modified polyester thread adsorbed with copper ions was treated with 0.05 mol / L potassium borohydride solution for 120 s to obtain a polyester thread evenly attached to the metallic copper activation catalyst layer.

[0058] (4) Dissolve 1.0g copper sulfate pentahydrate, 0.6g nickel sulfate hexahydrate, and 12.5g potassium sodium tartrate tetrahydrate in deionized water, then adjust the pH value of the solution with sodium hydroxide to obtain 500ml of dark blue with a pH value of 12.5 solution. Use a pipette to take 3ml...

Embodiment 3

[0062] (1) Pre-soak the polyester thread with a 15 g / L tannic acid solution at room temperature for 30 minutes, take out the polyester thread, wash it with deionized water three times, and dry it to obtain a tannic acid-modified polyester thread.

[0063] (2) Soak the tannic acid modified polyester thread in 75 g / L copper sulfate pentahydrate solution for 3 hours, take it out, and obtain the modified polyester thread adsorbing copper ions.

[0064] (3) The modified polyester thread adsorbed with copper ions was treated with 0.1 mol / L sodium borohydride solution for 30 seconds to obtain a polyester thread evenly attached to the metallic copper activation catalyst layer.

[0065] (4) Dissolve 5.0g copper sulfate pentahydrate, 0.3g nickel sulfate hexahydrate, and 15.0g potassium sodium tartrate tetrahydrate in deionized water, then adjust the pH value of the solution with sodium hydroxide to obtain 500ml of dark blue with a pH value of 12.5 solution. Take 4ml of 38% formaldehyde...

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Abstract

The invention relates to the technical field of metallic functional woven products, and particularly relates to a pretreatment method of conductive polyester fibers, the conductive polyester fibers and a preparation method thereof. The pretreatment method of the conductive polyester fibers comprises the following step: adsorbing a modifying agent on the polyester fibers to obtain modified polyester fibers, wherein the modifying agent is selected from plant polyphenol. According to the pretreatment method, the modifying agent is green and environmentally-friendly, the modifying agent is adsorbed to the surfaces of the polyester fibers through mutual static effect and hydrogen bond effect to form a supermolecule structural film layer which can be used as an interface layer between a metal coating and the polyester fibers, so that the bonding capacity between the metal coating and the polyester fibers can be improved, and no damage is caused to the performance of the polyester fibers; thedefects that the polyester fibers are damaged, and the performance of the fibers are destroyed, and the environmental pollution is caused in a traditional pretreatment method can be overcome. The pretreatment method is simple, easy to control, green and environmentally-friendly.

Description

technical field [0001] The invention relates to the technical field of metallized functional textiles, in particular to a pretreatment method for conductive polyester fibers, conductive polyester fibers and a preparation method thereof. Background technique [0002] Metallized conductive fiber combines the characteristics of fiber and metal. Compared with other conductive fibers, it has the advantages of small specific gravity and good conductivity, and its good flexibility and cohesion make it flexible and reprocessable. It is blended with ordinary fibers into yarn, and further made into fabrics as conductive, antistatic and electromagnetic shielding materials, which can significantly improve the material's hand feel and air permeability, and reduce the cost of materials. Metallized conductive fibers are widely used in antistatic, electromagnetic shielding, heat radiation resistance, antibacterial, sensors and smart textiles and other fields. [0003] The electroless plati...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M13/238D06M13/152D06M15/13D06M11/83D06M11/80D06M101/32
CPCD06M11/80D06M11/83D06M13/152D06M13/238D06M15/13D06M2101/32D06M2200/35D06M2200/50
Inventor 董智贤曾润鹏
Owner GUANGDONG UNIV OF TECH
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