Lactose-free milk preparation method based on separation membrane technologies

A lactose-free and membrane-separating technology, applied in dairy products, milk preparations, applications, etc., can solve the problems of easy inactivation of enzymes, difficult recovery of lactase, and high cost of enzymes

Pending Publication Date: 2019-05-14
ZHEJIANG UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the lactose-free milk on the market is basically obtained by enzymatic hydrolysis of lactose. However, due to the high cost of the enzyme, and the difficulty of recovering the free lactase, the enzyme is easily inactivated and other disadvantages.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Step 1: 968g of milk after pasteurization is carried out 5 times of dialysis to remove fat components through the PVC hollow fiber membrane with molecular weight cut-off of 100KDa. The obtained retentate was diluted with 738g of deionized water, and then passed through the PVC hollow fiber membrane for the next dialysis, wherein the milk was not diluted during the first dialysis (during the first 4 times of dialysis, each dialysis obtained about 200g of retentate ); combine the permeate obtained from 1~5 times of dialysis (the total amount of the combined permeate is 3256.8g), and obtain relatively small substances containing whey protein, lactose, inorganic salts, small molecule cellulose, dietary fiber, etc. The first permeate; collect the retentate 662g obtained after the 5th dialysis, which is the first retentate containing fat and casein micelles;

[0023] Step 2: the 3256.8g first permeated liquid obtained in step 1 is used to carry out 4 times of dialysis interce...

Embodiment 2

[0029] Step 1: 1936g of milk after pasteurization is carried out 5 times of dialysis to remove fat components through the PVC hollow fiber membrane with molecular weight cut-off of 100KDa. The obtained retentate was diluted with 1438g of deionized water, and then passed through the PVC hollow fiber membrane for the next dialysis, wherein the milk was not diluted during the first dialysis (during the first 4 times of dialysis, each dialysis obtained about 400g of retentate ); combine the permeate obtained from 1~5 times of dialysis (the total amount of permeate combined is 7018.6g), and obtain relatively small substances containing whey protein, lactose, inorganic salts, small molecular cellulose, dietary fiber, etc. The first permeate; collect 663.4g of the retentate obtained after the 5th dialysis, which is the first retentate containing fat and casein micelles;

[0030] Step 2: the 7018.6g first permeated liquid obtained in step 1 is used to carry out 4 times of dialysis to ...

Embodiment 3

[0036] Step 1: 4840g of milk after pasteurization is carried out 5 times of dialysis to remove fat component through the PVC hollow fiber membrane of 100KDa molecular weight cut-off, when described milk is carried out first 4 times of dialysis by PVC hollow fiber membrane, each dialysis The obtained retentate was diluted with 3878g deionized water, and then passed through the PVC hollow fiber membrane for the next dialysis, wherein the milk was not diluted during the first dialysis (during the first 4 times of dialysis, each dialysis obtained about 1000g of retentate ); combine the permeate obtained from 1~5 times of dialysis (the combined total amount of permeate is 18684.5g), and obtain relatively small substances containing whey protein, lactose, inorganic salts, small molecule cellulose, dietary fiber, etc. The first permeate; collect the retentate 1662g obtained after the 5th dialysis, which is the first retentate containing fat and casein micelles;

[0037] Step 2: the 1...

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PUM

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Abstract

The invention discloses a lactose-free milk preparation method based on separation membrane technologies, in which the four membrane technologies of microfiltration, ultrafiltration, electrodialysis and nanofiltration are coupled. The method includes the steps that firstly, most components in milk are intercepted through microfiltration and ultrafiltration, a penetrating solution is an aqueous solution containing lactose and inorganic salt, and after the inorganic salt is recovered by electrodialysis, desalinated liquid containing lactose and a small amount of inorganic salt is obtained; then,the desalinated liquid is subjected to nanofiltration separation to intercept lactose, and thus lactose removal is completed; components except lactose are recombined to obtain lactose-free milk powder through spray drying. By means of the method, the lactose interception rate reaches up to 95.85%; the production of the lactose-free milk powder is realized; meanwhile, water added in the production process can be effectively recovered and reused, lactose is also recovered by nanofiltration, and thus the method can guarantee that the whole process is environmentally friendly and free of by-product generation and raw material waste; besides, no chemical substance is added in the process, and thus the taste of milk will not be affected.

Description

technical field [0001] The invention relates to a method for preparing lactose-free milk based on separation membrane technology. Background technique [0002] Milk is rich in protein and minerals, and milk is the best source of calcium for the human body, known as "white blood". However, the presence of lactose in milk is extremely inconvenient for most people who are lactose intolerant. Because the patient's intestinal tract cannot secrete the enzyme that breaks down lactose, the lactose is digested and absorbed for use by the human body. Lactose will be decomposed by bacteria in the intestinal tract into lactic acid, thereby destroying the alkaline environment of the intestinal tract, and causing the intestinal tract to secrete a large amount of alkaline digestive juice to neutralize the lactic acid. So prone to mild diarrhea. The lactose-free milk currently on the market is basically obtained by enzymatic hydrolysis of lactose. However, due to the high cost of the enz...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23C9/142A23C9/144
Inventor 潘杰峰张宏杰沈江南赵雪婷
Owner ZHEJIANG UNIV OF TECH
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