A kind of medicine for tumor treatment and its preparation method and application
A tumor treatment and drug technology, applied in the field of tumor treatment drugs and its preparation, can solve the problems of difficult to reach deep lesion areas, low gas controllable release efficiency, etc., achieve good acid responsiveness, good biological safety, and prolong survival the effect of time
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Embodiment 1
[0036] Preparation of materials: firstly H 2 O (120ml), MgB 2 (90mg), PEG (4000) (450mg) were mixed uniformly in the container, placed on ice bath, and added H 2 o 2 (9ml) and HAc (180ul), and then use an ultrasonic breaker to break the glass. The parameters of the ultrasonic breaker are set as follows: the horn is 6, (intermittent time) 2.2s / (working time) 6.6s, and a total of 60 minutes of ultrasonication. After the ultrasonic crushing is completed, immediately divide into 50ml centrifuge tubes for centrifugation (12500r / s, 25min), and wash the obtained precipitate twice with water (12500r / s, 25min) and with absolute ethanol twice (12500r / s, 10min). . The final precipitate was vacuum-dried for 5 h to obtain novel two-dimensional magnesium boride nanosheets MBNs.
[0037] figure 1 It is the transmission electron microscope (TEM) and scanning electron microscope (SEM) images of the material, indicating that the MBNs material prepared above is a network structure of two-di...
Embodiment 2
[0040] To detect the toxicity of hydrogen gas combined with chemotherapy drug DOX on cancer cells and normal cells and the effect on ATP production. The cells selected were gastric cancer cells (BGC-823) and four normal cells (H9C2, LO2, mMSC, HEK-293 cells). And each cell was divided into air group, air+DOX (1 μg / mL, 0.5 μg / mL, 0.25 μg / mL, 0.125 μg / mL), hydrogen group, hydrogen+DOX (1 μg / mL, 0.5 μg / mL, 0.25μg / mL, 0.125μg / mL) groups to detect the attenuation and synergistic effect of hydrogen on chemotherapy drugs, in which hydrogen group, hydrogen + DOX (1μg / mL, 0.5μg / mL, 0.25μg / mL, 0.125μg / mL ) group, cultivated in a special hydrogen incubator containing 60%. Image 6 Demonstrated the attenuation and synergistic effect of hydrogen on chemotherapy drugs at the cellular level, the results showed that the DOX concentration (1 μg / mL, 0.5 μg / mL, 0.25 μg / mL, 0.125 μg / mL) damages cancer cells with The increase of DOX concentration increases, and it also has the same damage pattern...
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