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Solid Lubricant Polysaccharide Derivatives for Drilling Fluid

A solid lubricant and drilling fluid technology, applied in the direction of drilling compositions, chemical instruments and methods, etc., can solve the problems of unprepared, etc., and achieve the effect of easy biodegradation, stable properties and good lubricating performance

Active Publication Date: 2020-09-29
石家庄华莱鼎盛科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This technology does not produce polysaccharide derivatives in the traditional sense, but only solid lubricants

Method used

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  • Solid Lubricant Polysaccharide Derivatives for Drilling Fluid
  • Solid Lubricant Polysaccharide Derivatives for Drilling Fluid

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Embodiment 1: The solid lubricant polysaccharide derivative for drilling fluid of the present invention is made from the raw materials of following weight ratio: 30 parts of hydroxypropyl guar gum, 3 parts of propylene oxide, 0.1 parts of sodium hydroxide 20 parts of dodecyl alcohol, 0.15 parts of sulfuric acid catalyst, 10 parts of white oil, 2.5 parts of surfactant, 1 part of defoamer, 10 parts of mica powder, 1 part of bactericide, 6 parts of ethanol, and 20 parts of water; Described white oil is the combination of No. 7 white oil and No. 10 white oil two kinds of raw materials, and its weight ratio is 1: 1; Described catalyst sulfuric acid is the sulfuric acid aqueous solution that molar concentration is 0.1mol / L; Described surface Active agent is the combination of two kinds of raw materials of OP-10 surfactant and AEO-9 surfactant, and the weight ratio of OP-10 surfactant and AEO-9 surfactant is 1: 1.5; Described defoamer It is polyoxyethylene oxypropylene glyceri...

Embodiment 2

[0022] Embodiment 2: The solid lubricant polysaccharide derivative for drilling fluid of the present invention is made from the raw materials of following weight ratio: 40 parts of hydroxypropyl guar gum, 4 parts of propylene oxide, 0.15 parts of sodium hydroxide 25 parts of dodecyl alcohol, 0.2 parts of phosphoric acid catalyst, 12 parts of white oil, 3 parts of surfactant, 2 parts of defoamer, 12 parts of mica powder, 2 parts of bactericide, 8 parts of ethanol, and 10 parts of water; Described white oil is the combination of No. 7 white oil and No. 10 white oil, and the weight ratio of No. 7 white oil and No. 10 white oil is 1: 2; Described catalyst phosphoric acid is the phosphoric acid that molar concentration is 0.1mol / L aqueous solution; the surfactant is OP-10 surfactant; the defoamer is polydimethylsiloxane; the fungicide is starch preservative DL-D401.

[0023] The preparation method of the described solid lubricant polysaccharide derivative for drilling fluid compris...

Embodiment 3

[0024] Embodiment 3: the solid lubricant polysaccharide derivative for drilling fluid of the present invention is made from the raw materials of following weight ratio: 32 parts of hydroxypropyl guar gum, 3 parts of propylene oxide, 0.15 parts of sodium hydroxide 20 parts of dodecyl alcohol, 0.15 parts of catalyst, 15 parts of white oil, 3 parts of surfactant, 2 parts of defoamer, 10 parts of mica powder, 2 parts of bactericide, 8 parts of ethanol, and 18 parts of water; White oil is the combination of No. 7 white oil and No. 10 white oil, and the weight ratio of No. 7 white oil and No. 10 white oil is 1: 2; Described catalyzer is the combination of two kinds of raw materials of hydrochloric acid and sulfuric acid, and its weight ratio is 1: 1, described hydrochloric acid is the hydrochloric acid aqueous solution that molar concentration is 0.1mol / L, and described sulfuric acid is the sulfuric acid aqueous solution that molar concentration is 0.1mol / L; Described tensio-active a...

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Abstract

The invention relates to a solid lubricant glycan derivative for a drilling fluid. Raw materials of the derivative comprise, 30-40 parts of hydroxypropyl guanidine gum, 3-4 parts of propylene epoxide,0.1-0.15 part of sodium hydroxide, 20-30 parts of dodecyl alcohol, 0.15-0.2 part of a catalyst, 10-20 parts of white oil, 2-5 parts of a surfactant, 0.1-2 parts of an antifoaming agent, 10-20 parts of mica powder, 1-3 parts of a bactericide, 6-10 parts of ethanol and 10-25 parts of water. A preparation method includes the steps that the hydroxypropyl guanidine gum, the sodium hydroxide and the water are added into a reaction still and stirred continuously, and the propylene epoxide is added for stirring, refluxing and a reaction; a reaction solution is heated, the catalyst is added, and a mixed solution of the ethanol and the dodecyl alcohol is added under stirring for a reaction; the reaction material solution is cooled to the room temperature, the white oil, the surfactant, the antifoaming agent, the mica powder and the bactericide are added, stirred uniformly, dried and ground into powder, and then the derivative is obtained. The lubricating coefficient reduction rate is higher than or equal to 90%, the derivative has good high-temperature drop reduction performance and salt resistance, the preparation conditions are easily achieved, and the derivative is environmentally friendly.

Description

technical field [0001] The invention relates to a petroleum drilling fluid additive, in particular to a solid lubricant polysaccharide derivative for drilling fluid. The invention also relates to a preparation method of the polysaccharide derivative of the solid lubricant for drilling fluid. Background technique [0002] Drilling fluid lubricant is one of the main treatment agents for drilling fluid. It is mainly used to reduce the friction between the drilling tool and the well wall, so as to effectively avoid the occurrence of downhole accidents such as pipe sticking. In recent years, with the emergence of complex well structures such as deep wells, ultra-deep wells, and extended-reach wells, the conditions of high friction, high torque, and high temperature in drilling have put forward higher requirements for the lubricating performance of lubricants used in drilling fluids. At the same time, as the world's environmental protection requirements become increasingly string...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/035C08B37/00
CPCC08B37/00C09K8/035C09K2208/02C09K2208/28C09K2208/34
Inventor 陈利赵秀平
Owner 石家庄华莱鼎盛科技有限公司
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