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A shell-based fruit and vegetable cleaning agent and its preparation method and application method

A fruit and vegetable cleaning agent and shell technology, applied in the field of cleaning agents, can solve the problems of long time-consuming and single effect for removing pesticides, and achieve the effects of large-scale industrial production and application, obvious effect, and simple and fast use.

Active Publication Date: 2021-07-30
WUYI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, shell powder fruit and vegetable cleaning agents in the market are generally prepared by physically mixing surfactants and calcium hydroxide shell powder, which takes a long time to remove pesticides and has a single effect

Method used

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  • A shell-based fruit and vegetable cleaning agent and its preparation method and application method
  • A shell-based fruit and vegetable cleaning agent and its preparation method and application method
  • A shell-based fruit and vegetable cleaning agent and its preparation method and application method

Examples

Experimental program
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Effect test

Embodiment 1

[0049] A shell-based fruit and vegetable cleaning agent, comprising the following components in percentage by weight: 90% calcined shell powder, 0.15% peppermint oil, 0.25% calcium chloride, 1.3% citric acid, 1.2% sodium α-olefin sulfonate %, sodium citrate 3.5%, polysorbate 80 2.4% and lecithin 1.2%; the shells are clams, mussel shells and scallop shells with a mass ratio of 1.5:1.1:2.0.

[0050] Calcined shell powder is prepared by the following method:

[0051] Soak the shells with 0.7% hydrochloric acid for 45 minutes, and dry them at 120°C for 2 hours;

[0052] The dried shells were crushed to 90 mesh, and then calcined under a nitrogen atmosphere at a temperature of 950°C, a heating rate of 10°C / min, and a calcining time of 70 minutes to obtain calcined shell powder.

[0053] The preparation method of the fruit and vegetable cleaning agent: crush calcined shell powder to 200 mesh, soak in water for 8 hours, add citric acid, sodium α-olefin sulfonate, sodium citrate, polys...

Embodiment 2

[0067] A shell-based fruit and vegetable cleaning agent, comprising the following components by weight percentage: 85% calcined shell powder, 0.1% lemon oil, 0.3% calcium chloride, 1.5% citric acid, 1.9% sodium α-olefin sulfonate, Sodium citrate 5.6%, polysorbate 80 3.7% and lecithin 1.9%; shells are clams, mussel shells and scallop shells with a mass ratio of 1:1.5:1.5.

[0068] Calcined shell powder is prepared by the following method:

[0069] Soak the shells in 0.6% hydrochloric acid for 60 minutes, and dry them at 110°C for 3 hours;

[0070] The dried shells were crushed to 100 mesh, and then calcined under a nitrogen atmosphere at a temperature of 900°C, a heating rate of 8°C / min, and a calcining time of 80 minutes to obtain calcined shell powder.

[0071] The preparation method of the fruit and vegetable cleaning agent: crush calcined shell powder to 200 mesh, soak in water for 6 hours, add citric acid, sodium α-olefin sulfonate, sodium citrate, polysorbate 80 and leci...

Embodiment 3

[0073] A shell-based fruit and vegetable cleaning agent, comprising the following components in weight percentage: 92% calcined shell powder, 0.2% citrus oil, 0.2% calcium chloride, 1.2% citric acid, 0.9% sodium α-olefin sulfonate , sodium citrate 2.8%, polysorbate 80 1.8% and lecithin 0.9%; shells are clams, mussel shells and scallop shells with a mass ratio of 2:1:1.5.

[0074] Calcined shell powder is prepared by the following method:

[0075] Soak the shells with 0.8% hydrochloric acid for 30 minutes, and dry them at 130°C for 1 hour;

[0076] The dried shells were crushed to 80 meshes, and then calcined under a nitrogen atmosphere at a temperature of 1000° C., a heating rate of 15° C. / min, and a calcination time of 50 minutes to obtain calcined shell powder.

[0077] The preparation method of the fruit and vegetable cleaning agent: crush calcined shell powder to 180 mesh, soak in water for 7 hours, add citric acid, sodium α-olefin sulfonate, sodium citrate, polysorbate 8...

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Abstract

The invention discloses a shell-based fruit and vegetable cleaning agent and its preparation method and application method. The shell-based fruit and vegetable cleaning agent comprises the following components in weight percentage: 85-92% of calcined shell powder, 0.1-0.2% of essence %, calcium chloride 0.2‑0.3%, citric acid 1.2‑1.5%, and the rest are additives. Soak the shells with hydrochloric acid and dry them; crush the dried shells, and then calcinate them under a nitrogen atmosphere to obtain calcined shell powder; pulverize the calcined shell powder, soak them in water, add citric acid and additives, and filter , take the precipitate, dry it, add calcium chloride and essence to obtain the fruit and vegetable cleaning agent. The fruit and vegetable cleaning agent of the invention can effectively remove pesticides and heavy metal ions on the surface of fruits and vegetables, is harmless to human bodies and the environment, is simple to prepare, does not require complex mechanical equipment, and is easy to realize industrialized production.

Description

technical field [0001] The invention belongs to the field of cleaning agents, and in particular relates to a shell-based fruit and vegetable cleaning agent and a preparation method and an application method thereof. Background technique [0002] In the process of agricultural production, in order to reduce insect pests and promote the growth of fruits and vegetables, most agricultural products will inevitably be sprayed with appropriate chemical or biological pesticides (mostly organochlorine or organophosphorus) during the growth process, making the problem of pesticide residues in fruit and vegetable products more serious. Long-term accumulation of pesticides in the human body will cause chronic poisoning of the human body, and in severe cases, it will lead to neurological dysfunction, slow response and other poisoning symptoms. [0003] At present, the commonly used methods of cleaning fruits and vegetables include boiling water treatment, ultraviolet light irradiation, f...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11D1/83C11D3/04C11D3/20C11D3/12C11D3/36C11D3/382C11D3/384C11D11/00C11D3/60
CPCC11D1/83C11D3/046C11D3/2086C11D3/12C11D3/362C11D3/382C11D3/384C11D1/14C11D1/667C11D2111/10
Inventor 薛晓武卿宁
Owner WUYI UNIV