A method for preparing silicon carbide nanowire-reinforced titanium matrix composites at low temperature
A technology of silicon carbide nanowires and titanium-based composite materials, which is applied in the directions of silicon carbide, carbide, nanotechnology, etc., can solve the problems of weakening the toughening effect of silicon carbide nanowires and losing the structural characteristics of silicon carbide nanowires. Guarantee the effect of strengthening and toughening, improve the effect of strengthening and toughening, and improve the mechanical properties
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Embodiment 1
[0036] This embodiment includes the following steps:
[0037]Step 1, mix absolute ethanol and tetraethyl orthosilicate and stir evenly, then add distilled water and a hydrochloric acid solution with a mass concentration of 37% and stir uniformly to obtain a silica sol; the absolute ethanol, tetraethyl orthosilicate , The molar ratio of hydrochloric acid in distilled water and hydrochloric acid solution is 3:0.5:3:0.1;
[0038] Step 2. Add graphite powder with a particle size of 60 mesh to 150 mesh to the silica sol obtained in step 1 and stir for 20 minutes, then place it in an oven, and dry it for 12 hours at a temperature of 100°C to obtain a coated silica sol. Graphite powder of silica sol; the mass ratio of graphite powder to silica sol with a particle size of 60 mesh to 150 mesh is 1:5;
[0039] Step 3, placing the graphite powder coated with silica sol obtained in step 2 in a high-temperature tube furnace for carbothermal reduction reaction, and then undergoing an ultra...
Embodiment 2
[0059] This embodiment includes the following steps:
[0060] Step 1, mix absolute ethanol and tetraethyl orthosilicate and stir evenly, then add distilled water and a hydrochloric acid solution with a mass concentration of 37% and stir uniformly to obtain a silica sol; the absolute ethanol, tetraethyl orthosilicate , The molar ratio of hydrochloric acid in distilled water and hydrochloric acid solution is 5:2:8:0.5;
[0061] Step 2. Add graphite powder with a particle size of 60 mesh to 150 mesh into the silica sol obtained in step 1 and stir for 60 minutes, then place it in an oven, and dry it for 24 hours at a temperature of 100°C to obtain a coated silica sol. Graphite powder of silica sol; the mass ratio of graphite powder to silica sol with a particle size of 60 mesh to 150 mesh is 1:5;
[0062] Step 3, placing the graphite powder coated with silica sol obtained in step 2 in a high-temperature tube furnace for carbothermal reduction reaction, and then undergoing an ultr...
Embodiment 3
[0066] This embodiment includes the following steps:
[0067] Step 1, mix absolute ethanol and tetraethyl orthosilicate and stir evenly, then add distilled water and a hydrochloric acid solution with a mass concentration of 37% and stir uniformly to obtain a silica sol; the absolute ethanol, tetraethyl orthosilicate , The molar ratio of hydrochloric acid in distilled water and hydrochloric acid solution is 4:1.5:6:0.3;
[0068] Step 2. Add graphite powder with a particle size of 60 mesh to 150 mesh into the silica sol obtained in step 1 and stir for 40 minutes, then place it in an oven, and dry it for 20 hours at a temperature of 100°C to obtain a coated silica sol. Graphite powder of silica sol; the mass ratio of graphite powder to silica sol with a particle size of 60 mesh to 150 mesh is 1:5;
[0069] Step 3, placing the graphite powder coated with silica sol obtained in step 2 in a high-temperature tube furnace for carbothermal reduction reaction, and then undergoing an ul...
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