A hybrid gel particle plugging agent while drilling and its preparation method
A hybrid gel and plugging technology while drilling, which is applied in the field of drilling fluid plugging, can solve problems such as insufficient binding force, heterogeneous gel, poor dispersion and compatibility, etc., and achieve high pressure bearing capacity and toughness Strong, enhanced bond strength
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Embodiment 1
[0043] A hybrid gel particle LWD plugging agent, prepared from the following raw materials in parts by mass: 20 parts of reactive monomers, 1.0 parts of crosslinking agent, 0.3 parts of initiator, 3.0 parts of silane coupling agent, nano-scale Rigid particles 1.0 parts.
[0044] The reactive monomer is methacrylamide, hydroxyethyl methacrylate and sodium p-styrenesulfonate, the mass ratio is 5:2:1; the crosslinking agent is hydroxypropyl methacrylate; the initiator is azobis Isobutylamidine hydrochloride (AIBA, V-50); silane coupling agent is KH550 (3-aminopropyltriethoxysilane); nano-scale rigid particles are nano-silica (average particle size 20±3nm , density 2.3g / cm 3 ).
[0045] The preparation method of the above-mentioned hybrid gel particle plugging agent while drilling comprises the steps of:
[0046] (1) Firstly, dissolve the silane coupling agent in deionized water to configure coupling agent solution A (the mass ratio of silane coupling agent to deionized water i...
Embodiment 2
[0052] A hybrid gel particle LWD plugging agent, prepared from the following raw materials in parts by mass: 20 parts of reactive monomers, 1.0 parts of crosslinking agent, 0.3 parts of initiator, 3.0 parts of silane coupling agent, nano-scale Rigid particles 1.0 parts.
[0053] The reactive monomer is methacrylamide, hydroxyethyl methacrylate and sodium p-styrenesulfonate, the mass ratio is 4:2:1; the crosslinking agent is hydroxypropyl methacrylate; the initiator is azobis Isobutylamidine hydrochloride (AIBA, V-50); silane coupling agent is KH550 (3-aminopropyltriethoxysilane); nano-scale rigid particles are nano-silica (average particle size 20±3nm , density 2.3g / cm 3 ).
[0054] The preparation method of the above-mentioned hybrid gel particle plugging agent while drilling comprises the steps of:
[0055] (1) Firstly, dissolve the silane coupling agent in deionized water to configure coupling agent solution A (the mass ratio of silane coupling agent to deionized water i...
Embodiment 3
[0061] A hybrid gel particle LWD plugging agent, prepared from the following raw materials in parts by mass: 30 parts of reactive monomers, 1.0 parts of crosslinking agent, 0.4 parts of initiator, 3.0 parts of silane coupling agent, nano-scale Rigid particles 1.0 parts.
[0062] The reactive monomer is methacrylamide, hydroxyethyl methacrylate and sodium p-styrenesulfonate, the mass ratio is 4:2:1; the crosslinking agent is hydroxypropyl methacrylate; the initiator is azobis Isobutylamidine hydrochloride (AIBA, V-50); silane coupling agent is KH550 (3-aminopropyltriethoxysilane); nano-scale rigid particles are nano-silica (average particle size 20±3nm , density 2.3g / cm 3 ).
[0063] The preparation method of the above-mentioned hybrid gel particle plugging agent while drilling comprises the steps of:
[0064] (1) Firstly, dissolve the silane coupling agent in deionized water to configure coupling agent solution A (the mass ratio of silane coupling agent to deionized water i...
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