A cardiovascular stent for rapidly promoting vascular endothelialization and preparation method thereof
A cardiovascular and vascular technology, applied in the field of rapidly promoting vascular endothelialization of a cardiovascular stent and its preparation, can solve the problems of breaking the vascular homeostasis, increasing vasoconstrictor factors, reducing vasodilator factors, etc., and achieves the effect of promoting anticoagulation, The effect of promoting vascular endothelialization and uniform particle size
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preparation example Construction
[0043] The preparation method of the above-mentioned copper-zinc-magnesium-doped silicon-based mineral powder includes:
[0044] (1) First, add methanol and deionized water into the reactor, then add catalyst concentrated hydrochloric acid and stir evenly, and measure the pH between 0.8-1.3.
[0045] (2) Then, trialkoxysilane was added dropwise, and after the dropwise addition was completed, the reaction was stirred at 30-50° C. for 6-8 hours to carry out the hydrolysis reaction.
[0046] (3) Then, add copper-containing salts, zinc-containing salts, and magnesium-containing salts, and stir and react at 60-80 ° C for 4-8 h to promote the polycondensation of the hydrolyzate to form polyhedral cage-type polysilsesquioxane, and make it with Mix the salt evenly.
[0047] (4) The reaction product was distilled under reduced pressure to remove methanol, and the obtained product was placed to age for 48h.
[0048] (5) Spread the aged product in an oven at 100-120 degrees and bake fo...
Embodiment 1
[0074] The preparation method of the cardiovascular stent for rapidly promoting vascular endothelialization of the present embodiment includes the following steps:
[0075] (1) Powder preparation: The bioactive mineral material, Regesi regenerated silicon V-type produced by Beijing Happiness Probiotics, was screened, and then dried at 120 °C to form powder particles with a particle size of 300 nm.
[0076] (2) stent preparation: the medical stainless steel stent substrate is polished with different surface roughness, the surface roughness reaches 0.1, and then sterilized with a γ-ray Co60 irradiation dose of 20-35kGy for use.
[0077] (3) Supersonic cold spraying: using supersonic cold spraying, the above-mentioned powder particles enter the supersonic accelerated airflow at an off-axis of 45°, and the powder feeding flow rate is 0.5g / min to form a gas-solid two-phase flow. Impacted and deposited on the surface of the cardiovascular stent to form a coating, the bioactive miner...
Embodiment 2
[0083] The preparation method of the cardiovascular stent for rapidly promoting vascular endothelialization of the present embodiment includes the following steps:
[0084] (1) Powder preparation: The bioactive mineral material adopts the Regesi active silicon V type produced by Beijing Happiness Probiotics, and the operation method is the same as that of Example 1 to form powder particles with a particle size of 300 nm.
[0085] (2) Scaffold preparation: The scaffold substrate and the operation method in this step are the same as in Example 1, and the surface roughness of the scaffold substrate is 0.1.
[0086] (3) Supersonic cold spraying: using supersonic cold spraying, the above-mentioned powder particles enter the supersonic accelerated airflow at an off-axis of 40°, and the powder feeding flow rate is 1g / min to form a gas-solid two-phase flow, which is impacted at 150 °C , and deposited on the surface of the cardiovascular stent to form a coating, the bioactive mineral m...
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