A kind of white carbon black/natural rubber composite material preparation method
A technology of natural rubber and composite materials, applied in the field of continuous preparation of silica/natural rubber composite materials, can solve problems such as affecting the health of operators, lag in vulcanization time, affecting the performance of rubber products, etc., to achieve physical properties and dynamic performance. The effect of improved mechanical properties, shortened production cycle, and continuous processing methods
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Embodiment 1
[0015] The preparation method of the silica / natural rubber composite material involved in this embodiment is a high-temperature atomization method, and the process includes four steps of preparing an aqueous solution of silica, preparing an aqueous solution of auxiliary agents, preparing a silica masterbatch, and continuous mixing:
[0016] (1) Preparation of white carbon black aqueous solution: add 40 parts by mass of SiO in No. 1 beaker 2 (silicon dioxide), 5 parts by mass of liquid Si69 (silane coupling agent) solution and deionized water are mixed with 25wt% white carbon black aqueous solution, and the white carbon black aqueous solution is placed in an ultrasonic oscillator with a frequency of 1000 Hz for ultrasonic 10min, Then the solution after the ultrasonic wave is placed in a planetary ball mill for secondary crushing and grinding for 4 hours;
[0017] (2) Preparation of auxiliary agent aqueous solution: add 20 parts by mass of SiO in No. 2 beaker 2 (silicon dioxide...
Embodiment 2
[0021] This example involves the comprehensive performance test of silica / natural rubber composite material vulcanized rubber. The silica / natural rubber composite material will be prepared by using smoked sheet glue-dry method, acid flocculation method-wet method and high temperature atomization method respectively. Prepare into sizing material, wherein, the preparation process of high-temperature atomization method sizing material is: the white carbon black / natural rubber composite material prepared in step (4) and 1 mass part S (sulfur) and 1.2 mass parts CZ (N-ring Hexyl-2-benzothiazole sulfenamide) is placed in the mill and passed through 6 times to obtain the sizing material; three parts of the sizing material are tested for mechanical properties respectively, and the results are as follows:
[0022]
[0023]
[0024] According to the data of tensile strength and tear strength, it can be seen that the rubber compound prepared by high temperature atomization method has ...
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