Graphene reinforced and toughened biodegradable polyester compound and foaming material thereof
A technology for strengthening, toughening, and degrading polyester, which is used in biological packaging, sustainable packaging, climate sustainability, etc. It can solve the problem of low foaming material ratio, poor compatibility, physical foaming behavior, and limited improvement in material toughness. and other problems to achieve the effect of improving physical foaming behavior, increasing tensile strength and elongation at break, and improving compatibility
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Embodiment 1
[0022] Disperse 1 g of graphene oxide (with a carbon-to-oxygen ratio of 3, containing epoxy groups, carboxylic acid groups, and aldehyde groups) in 500 ml of water through a high-energy ultrasonic probe, and freeze-dry the GO aqueous solution to obtain fluffy GO powder. 1 g of GO powder was dispersed in 50 g of DMF. Dissolve 5 g of the trifunctional epoxy chain extender in 30 ml of DMF by stirring, add the resulting dispersion into the GO / DMF dispersion, and continue stirring for 2 h. A triphenylphosphine catalyst is added to the dispersion to induce a chemical reaction. The epoxy-grafted GO (GO-epoxy) powder was obtained by multiple filtration, washing with acetone, and drying. PBAT (50% by weight), PLA (49% by weight) and GO-epoxy (1% by weight) dried at 70°C / 5h were circulated at 200°C for 10 minutes, and molded to obtain a thickness of 1.0 mm biodegradable composite sheet. The biodegradable composite was saturated under the condition of 15MPa / 130°C for 30min, and the bi...
Embodiment 2
[0028] The preparation method of epoxy-grafted GO (GO-epoxy) powder is the same as that of Example 1. PBAT (89.9% by weight), PLA (10% by weight), and GO-epoxy (0.1% by weight) dried at 70°C / 5h were mixed at 200°C for 10 minutes, and molded to obtain a thickness of 1.0 mm biodegradable composite sheet. The biodegradable composite was saturated under the condition of 20MPa / 135°C for 30min, and the biodegradable composite foam material was obtained through rapid pressure release.
[0029] Studies have shown that the tensile strength of the biodegradable composite is 33 MPa, and the elongation at break is 150%; the density of the biodegradable composite foam material is 0.08 g / cm 3 , the hardness is Shao C42, the cell size is 120.3mm, and the cell density is 1.1´10 8 piece / cm 3 ; The tensile strength of the composite foam material is 4.3MPa, and the elongation at break is 210%.
Embodiment 3
[0034] The preparation method of epoxy-grafted GO (GO-epoxy) powder is the same as that of Example 1. PBAT (50% by weight), PLA (45% by weight), and GO-epoxy (5% by weight) dried at 70°C / 5h were circulated at 200°C for 10 minutes, and molded to obtain a thickness of 1.0 mm biodegradable composite sheet. The biodegradable composite was saturated under the condition of 20MPa / 135°C for 30min, and the biodegradable composite foam material was obtained through rapid pressure release.
[0035] Studies have shown that the tensile strength of the biodegradable composite is 42 MPa, and the elongation at break is 350%; the density of the biodegradable composite foam material is 0.05 g / cm 3 , the hardness is Shao C55, the cell size is 102.3mm, and the cell density is 3.5´10 8 piece / cm 3 ; The tensile strength of the composite foam material is 6.5MPa, and the elongation at break is 380%.
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