Production device and process of nitro-sulfur-based water-soluble fertilizer

A production process and production device technology, applied in the field of production devices of nitrosulfur-based water-soluble fertilizers, can solve problems such as flatulence, poor water solubility, and hardening

Pending Publication Date: 2020-07-10
湖北省黄麦岭磷化工有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] (1) The production process is relatively backward
Compared with international water-soluble fertilizer companies, the current domestic water-soluble fertilizer production technology is relatively backward; in terms of research and development, the investment in funds and technical personnel is seriously insufficient, and the production equipment is very simple
Many enterprises simply mix urea with potassium nitrate, potassium sulfate, water-soluble monoammonium phosphate and other raw materials after crushing. There is no dehumidification equipment in the production workshop, and the dyeing and anti-caking technology is not good enough. The fertilizer produced often deliquescence , flatulence, hardening, uneven dyeing, excessive impurities, poor water solubility, etc., seriously affect the sales of products
[0007] (2) The formula concentration is unscientific
Many domestic manufacturers do not determine the concentration according to the nutrient requirements of different crops and crop growth periods when formulating product formula concentration, which makes it difficult to achieve the expected effect when using the product
Blindly produce water-soluble fertilizers with high nutrient content, and fail to produce water-soluble fertilizers with medium and low nutrient content according to actual needs
[0008] (3) The product price is super high
At present, no matter the agricultural standard or the chemical standard, there are no indicators and detection methods for the dissolution rate, which makes it impossible to supervise

Method used

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  • Production device and process of nitro-sulfur-based water-soluble fertilizer
  • Production device and process of nitro-sulfur-based water-soluble fertilizer
  • Production device and process of nitro-sulfur-based water-soluble fertilizer

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0045] The production device of nitrosulfur-based water-soluble fertilizer, mixing tank 1, phosphoric acid pipeline 2, sulfuric acid pipeline 3, liquid ammonia pipeline 4, washing liquid pipeline 5, and medium-pressure steam pipeline 6 are respectively connected to the tubular reactor 7 through pipelines, and the tubular reaction The device is arranged in the granulator 8, and the granulator 8 is connected to the nitrosulfur-based water-soluble fertilizer storage device. The mixing tank 1 is provided with a slurry feed pipe 9 , a low-pressure steam feed pipe 10 , a process water feed pipe 11 and a monoammonium phosphate feed pipe 14 . The granulator 8 is also provided with a granulator solid storage tank feed pipe 12 and a low-pressure steam feed pipe 10 .

Embodiment 2

[0047] A production process of nitrosulfur-based water-soluble fertilizer, characterized in that,

[0048] (1) Put the mixture of potassium salt, ammonium nitrate, and humic acid in a mass ratio of 1:1:0.3 as a solid raw material from the raw material system, and add it to the granulator;

[0049] (2) Pumping monoammonium phosphate, ammonium nitrate, process water, and low-pressure steam to the slurry storage tank to form a mass fraction of 66% monoammonium phosphate slurry, the moisture content of the monoammonium phosphate slurry is 22%, and the temperature is 110 ℃;

[0050] (3) Monoammonium phosphate slurry, ammonium nitrate phosphorus, washing liquid (the washing liquid comes from the washing liquid produced after the concentrated phosphoric acid is pumped into the tail washing system), concentrated phosphoric acid to form a blended slurry (the water content of the blended slurry is 14%, the temperature is 110°C, the mass ratio of the monoammonium phosphate slurry, ammon...

Embodiment 3

[0052] (1) Put the solid raw materials of potassium salt, ammonium nitrate and EDTA into the raw material system and add them into the granulator. The feed rate is 6.24t / h ammonium nitrate, 1.18t / h potassium chloride, 5.12t / h potassium sulfate, 0.98t / h chelating agent, and 0.105t / h zinc sulfate monohydrate.

[0053] (2) The flow rate of 66% monoammonium phosphate slurry is 2.21m 3 / h, 48%P 2 o 5 The flow rate of concentrated phosphoric acid is 1.65m 3 / h, 0.91t / h liquid ammonia and 2.67m 3 / h washing solution is pumped into the tubular reactor together.

[0054] (3) Spray the slurry in the tubular reactor to granulate in the granulator, and dry it under hot air at 125-250°C to prepare a 17-17-17 nitrosulfur-based water-soluble fertilizer. The pH value is 5.8-6.0.

[0055] The product quality indicators are obtained as follows:

[0056] 1. Total nitrogen 16.12%

[0057] 2. Ammonia nitrogen 11.92%

[0058] 3. Nitrate nitrogen 4.20%

[0059] 4. Total phosphorus 19.36% ...

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Abstract

The invention provides a production device and process of a nitro-sulfur-based water-soluble fertilizer. A mixing tank, a phosphoric acid pipeline, a sulfuric acid pipeline, a liquid ammonia pipeline,a washing liquid pipeline and a medium-pressure steam pipeline are respectively connected with a tubular reactor through pipelines, the tubular reactor is arranged in a granulator, and the granulatoris connected to a nitro-sulfur-based water-soluble fertilizer storage device. The preparation process comprises the following steps: feeding a mixture of potassium salt, ammonium nitrate phosphate and a chelating agent as a solid raw material from a raw material system, and adding the mixture into a granulator; pumping monoammonium phosphate, ammonium nitrate phosphate, process water and low-pressure steam into a slurry storage tank to form monoammonium phosphate slurry; and forming blended slurry from the monoammonium phosphate slurry, ammonium nitrate phosphate, a washing solution and concentrated phosphoric acid, pumping the blended slurry into a mixing tank, pumping the blended slurry into a tubular reactor after the blended slurry is formed, pumping sulfuric acid, liquid ammonia andsteam into the tubular reactor, spraying the slurry into the granulator for granulating, and performing drying to obtain the nitro-sulfur-based water-soluble fertilizer. The mass fraction of water-insoluble substances of the prepared nitro fertilizer can be stabilized to 0.2-0.3%.

Description

technical field [0001] The invention relates to a new water-soluble fertilizer, in particular to a production device and process of a nitrosulfur-based water-soluble fertilizer. Background technique [0002] Water-soluble fertilizers are chemical fertilizers that can be quickly and completely dissolved in water. It can be used for foliar spraying, drip irrigation, sprinkler irrigation, etc. It can be solid powder, solid granule, liquid clear night, liquid suspension, etc. [0003] Water-soluble fertilizers in the prior art have the following characteristics: [0004] [0005] At present, the main problems of water-soluble fertilizers in my country include the following: [0006] (1) The production process is relatively backward. Compared with international water-soluble fertilizer companies, the current domestic water-soluble fertilizer production technology is relatively backward; in terms of research and development, the investment in funds and technical personnel i...

Claims

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Application Information

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IPC IPC(8): C05G3/00C05G3/30C05G3/90
CPCC05B7/00C05C1/00C05D1/00C05F11/02C05D1/02C05D9/02C05C5/02
Inventor 王敬东李进梅亮贤刘锡平
Owner 湖北省黄麦岭磷化工有限责任公司
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