Method for rapidly preparing multi-dimensional fluorescent nanoparticles and quantitatively characterizing dynamic dispersion state of multi-dimensional fluorescent nanoparticles in situ
A fluorescent nanoparticle, dispersed state technology, used in fluorescence/phosphorescence, material analysis by optical means, measurement devices, etc., can solve the problem of difficulty in accurately distinguishing multidimensional fluorescent nanoparticle dispersion states, inability to monitor the evolution process, and lack of universality. Representation and other issues, to achieve the effect of fast test speed, reduced preparation difficulty, and enhanced curing uniformity
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[0022] Example 1
[0023] SiO for multi-dimensional nanoparticles 2 Nanoparticles and carbon nanotubes, fluorescein with aggregation-induced luminescence properties are selected from tetrastyrene-rhodamine B and tetrastyrene-fluorescein isothiocyanate, onium salt cationic light containing long-chain alkyl or alkoxy groups As the initiator, [4-(2-hydroxy-3-butoxy-1-propoxy)]phenylphenyliodonium-hexafluoroantimonate iodonium salt was used. Under darkroom conditions, anhydrous ethanol, SiO 2 Nanoparticles, tetrastyrene-rhodamine B, anhydrous ethanol, carbon nanotubes, and tetraphenylethylene-fluorescein isothiocyanate two groups of systems were mixed uniformly by ultrasonic stirring in a proportion of 100:0.2:0.01 according to the parts by mass. The ultrasonic power is 80kW, the stirring speed is 400r / min, and the time is 1h. After mixing uniformly, the precursor solution was poured into a light-tight tetrafluoro round-bottomed flask, which was placed in a closed microwave rea...
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[0026] Example 2
[0027] SiO for multi-dimensional nanoparticles 2 Nanoparticles and graphene oxide, fluorescein with aggregation-induced luminescence properties are selected from tetrastyrene-rhodamine B and tetrastyrene-7-amino-4-methylcoumarin, containing long-chain alkyl or alkoxyl groups. The onium salt type cationic photoinitiator adopts [4-(2-hydroxy-3-allyloxy-1-propoxy)]phenyl phenyl iodonium-hexafluoroarsenic acid iodonium salt. Under darkroom conditions, anhydrous ethanol, SiO 2 Nanoparticles, tetrastyrene-rhodamine B and anhydrous ethanol, graphene oxide, tetraphenylethylene-7-amino-4-methylcoumarin two groups of systems, in proportion to 100:1:0.05 according to the mass fraction Ultrasonic stirring respectively. The ultrasonic power is 120kW, the stirring speed is 800r / min, and the time is 1.5h. After mixing uniformly, the precursor solution was poured into a light-tight tetrafluoro round-bottomed flask, which was placed in a closed microwave reactor with a t...
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[0030] Example 3
[0031]Carbon nanotubes and graphene oxide are selected for multi-dimensional nanoparticles, and fluorescein with aggregation-induced luminescence properties is selected from tetrastyrene-fluorescein isothiocyanate and tetrastyrene-7-amino-4-methylcoumarin. Onium salt cationic photoinitiator of long-chain alkyl or alkoxy group adopts [4-(2-hydroxy-3-alkoxy-1-propoxy)]phenyl phenyl iodonium-hexafluorophosphate iodonium salt . Under darkroom conditions, two systems of absolute ethanol, carbon nanotubes, tetrastyrene-fluorescein isothiocyanate and absolute ethanol, graphene oxide, and tetrastyrene-7-amino-4-methylcoumarin were combined. , according to the mass ratio of 100:0.5:0.02, respectively, ultrasonically stir evenly. The ultrasonic power is 100kW, the stirring speed is 600r / min, and the time is 2h. After mixing uniformly, the precursor solution was poured into a light-tight tetrafluoro round-bottomed flask, which was placed in a closed microwave reacto...
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