Organic molybdenum lubricant composition trace lubricant and preparation method thereof

A lubricant composition and a technology for micro-lubricants, which are applied in the field of lubrication, can solve problems such as difficulty in machining metals that are difficult to process, and achieve the effects of remarkable environmental protection, excellent biodegradability, and good friction resistance.

Active Publication Date: 2020-08-04
SHANGHAI JINZHAO ENERGY SAVING TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] In these disclosed technologies, the organic molybdenum lubricant additive used is still relatively difficult to solve the processing of d...

Method used

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  • Organic molybdenum lubricant composition trace lubricant and preparation method thereof
  • Organic molybdenum lubricant composition trace lubricant and preparation method thereof
  • Organic molybdenum lubricant composition trace lubricant and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Weigh 1000g of laccarnation acid and 1000g of polyethylene glycol (PEG200) and place them in the reaction kettle, slowly add 80g of phosphorus pentoxide while stirring, after adding phosphorus pentoxide, fully stir the reaction at 120°C for 3 Hours, when the temperature drops below 100°C, add 200g of ammonium phosphomolybdate, heat to 150°C, fully react for 3 hours, remove moisture and ammonia under reduced pressure; cool down to below 100°C, add 100g of monoethanolamine and mix well; that is An organic molybdenum lubricant composition.

[0039] The above-prepared organic molybdenum lubricant composition and water are mixed and stirred evenly at a weight ratio of 1:2 and then used in a minimal quantity lubrication device.

Embodiment 2

[0041] Weigh 1000g of laccarnation acid and 500g of polyethylene glycol (PEG300) and place them in the reaction kettle, slowly add 50g of phosphorus pentoxide while stirring, after adding phosphorus pentoxide, fully stir the reaction at 130°C for 2 Hours, when the temperature drops below 100°C, add 150g of ammonium phosphomolybdate, heat to 160°C, fully react for 2 hours, remove moisture and ammonia under reduced pressure; cool down to below 100°C, add 80g of monoethanolamine and mix well; that is An organic molybdenum lubricant composition.

[0042] Weigh 300 g of organic molybdenum lubricant composition, 400 g of octyldodecyl myristate, 50 g of polycastor oil maleate, 100 g of castor oil sodium sulfonate, and 150 g of deionized water, mix and stir at room temperature until translucent It is a micro lubricant.

[0043] The preparation method of above-mentioned polycastor oil maleate:

[0044] Step 1: Add 933.43g (1 mol) of castor oil, 232.14 (2 mol) of maleic acid, and 5g o...

Embodiment 3

[0047] Weigh 1000g of laccarnation acid and 600g of polyethylene glycol (PEG400) and place them in the reaction kettle, slowly add 60g of phosphorus pentoxide while stirring, after adding phosphorus pentoxide, fully stir the reaction at 125°C for 2.5 Hours, when the temperature drops below 100°C, add 160g of ammonium phosphomolybdate, heat to 150°C, fully react for 3 hours, remove moisture and ammonia under reduced pressure; cool down to below 100°C, add 90g of monoethanolamine and mix well; that is An organic molybdenum lubricant composition.

[0048] Weigh 400 g of organic molybdenum lubricant composition, 300 g of octyldodecyl myristate, 100 g of polycastor oil maleate, 50 g of castor oil sodium sulfonate, and 150 g of deionized water, mix and stir at room temperature until translucent It is a micro lubricant.

[0049] The preparation method of above-mentioned polycastor oil maleate:

[0050] Step 1: Add 933.43g (1 mol) of castor oil, 116.07 (2 mol) of maleic acid, and 2g...

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Abstract

The invention provides an organic molybdenum lubricant composition which is characterized by being prepared from the following components in parts by weight: 100 parts of aleutric acid; 50-100 parts of polyethylene glycol; 15-20 parts of ammonium phosphomolybdate; 8-10 parts of monoethanolamine and 5-8 parts of phosphorus pentoxide. The organic molybdenum lubricant composition prepared by the invention is an extreme pressure and antiwear additive containing Mo-P-S-N, has excellent antifriction performance and is also a good surfactant. A trace lubricant containing the organic molybdenum lubricant composition is prepared from the following components in percentage by weight: 30 to 40 percent of the organic molybdenum lubricant composition; 30-40% of octyldodecyl myristate; 5-10% of castor oil polymaleate; 5-10% of sodium sulfonated castor oil and balance of deionized water. The micro lubricant prepared by the invention can meet the requirements of lubrication and cooling, extreme pressure and wear resistance and rust prevention in metal processing; and more than 90% of the lubricant can be saved when used with a micro lubricating device.

Description

technical field [0001] The invention belongs to the technical field of lubrication, and in particular relates to an organic molybdenum lubricant composition trace lubricant and a preparation method. Background technique [0002] The traditional metal cutting process uses mineral oil or vegetable oil or cutting fluid for a large amount of shower lubrication. The amount of lubricant used is large, which not only wastes resources, but also causes huge pollution to the processing site and the environment, and also seriously affects the health of the operators. . [0003] In order to solve these problems, some progress has been made in the research of micro-quantity lubrication technology recently. The micro-quantity lubrication technology solves the problems of large amount of lubricant used and serious pollution, but excessive use of sulfur and chlorine-containing additives that are not friendly to the environment , will have a certain impact on the environment. At the same t...

Claims

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Application Information

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IPC IPC(8): C10M141/10C10M173/02C10M177/00C10N40/22C10N30/06C10N30/12C10N10/02
CPCC10M141/10C10M173/02C10M177/00C10M2227/09C10M2215/082C10M2207/289C10M2223/04C10M2201/085C10M2201/02C10M2207/2815C10M2209/102C10M2219/044
Inventor 张乃庆吴启东蒋宁吴悠邱秋敏
Owner SHANGHAI JINZHAO ENERGY SAVING TECH
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