A method for strengthening and toughening non-ferrous metal materials

A non-ferrous metal strengthening and toughening technology, which is applied in the field of strengthening and toughening non-ferrous metal materials, can solve problems such as uneven size distribution, affecting product quality, and demanding processing technology, so as to improve solid solubility and solute atom diffusion ability , Improve the solid solution effect and surface quality, and promote the effect of solute atom diffusion

Active Publication Date: 2021-04-13
CENT SOUTH UNIV
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Problems solved by technology

The strength and plasticity of non-ferrous metal materials can be improved at the same time through grain refinement, but the extent to which grain refinement can improve the strength of alloys is limited. Therefore, to obtain higher-strength non-ferrous metal materials requires proper heat treatment to form a large amount of dispersion in the alloy. Realization of finely distributed reinforcement phase particles
[0003] At present, non-ferrous metal materials that can be strengthened by heat treatment are basically prepared by deformation heat treatment process, that is, "solution → processing → aging" process, in which solution treatment is annealed at a relatively high temperature for a long time, and there are the following problems: 1) Heating temperature High (0.9T s Above, T s is the melting point of the alloy), the holding time is long (depending on the batch size in the furnace, generally several hours), and the energy consumption is large; 2) The surface oxide layer is easy to form during the heat treatment process, and it is difficult to remove it in the subsequent process, which affects the product quality; 3) It is easy to cause abnormal growth of grains, resulting in coarse grains and uneven size distribution inside the alloy, which seriously damages the mechanical properties of the alloy; 4) The processing technology is demanding, and it is easy to cause uneven internal temperature of the material and local overburning, resulting in solid solution Poor uniformity, consistency and stability of alloy structure and properties after treatment
In addition, the alloy after solid solution treatment undergoes plastic forming and aging treatment. The aging temperature is generally lower than the recrystallization temperature. Although strengthening phases can be precipitated in the alloy to improve its strength, the solid solution treatment produces coarse grains and irregular size distribution. The homogeneous phenomenon still exists, and the plasticity of the prepared alloy is poor

Method used

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  • A method for strengthening and toughening non-ferrous metal materials
  • A method for strengthening and toughening non-ferrous metal materials
  • A method for strengthening and toughening non-ferrous metal materials

Examples

Experimental program
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Effect test

Embodiment 1

[0046] Embodiment 1: the preparation of H62 copper alloy strip

[0047] (1) The hot-rolled H62 (Cu-37.5wt% Zn) copper alloy strip blank is subjected to rapid solid solution and water spray cooling and quenching treatment by electric pulse, so that the precipitated phase in the alloy is solid-dissolved in the copper matrix. The electric pulse parameters input to the energized region of the copper alloy strip blank are: frequency 1500Hz, pulse width 100μs, current density amplitude 5000A / mm 2 , effective current density 700A / mm 2 , the maximum heating temperature is 800°C, the heating time is 30s; the cooling water flow rate of spray water is 50L / min.

[0048] (2) Carry out a cold rolling to the copper alloy strip material of electric pulse solution treatment in step (1), pass reduction rate 20%, total reduction rate 80%, rolling speed 50m / min;

[0049] (3) aging treatment is carried out to the primary cold-rolled copper alloy strip in step (2), the aging temperature is 450 DE...

Embodiment 2

[0063] Embodiment 2: Preparation of 7050 aluminum alloy strip

[0064] (1) Rapid solid solution and water spray cooling and quenching are carried out on the hot-rolled 7050 (Al-6.3wt% Zn-2.4wt% Cu-2.1wt% Mg) aluminum alloy strip by electric pulse, so that the precipitated phase in the alloy Soluble in aluminum matrix. The parameters of the electric pulse input to the energized area of ​​the aluminum alloy strip are: frequency 1000Hz, pulse width 120μs, current density amplitude 1500A / mm 2 , effective current density 250A / mm 2 , the maximum heating temperature is 420°C, the heating time is 15s; the flow rate of water spray cooling water is 30L / min.

[0065] (2) Carry out one-time cold rolling to the aluminum alloy strip material treated by electric pulse solution treatment in step (1), the pass reduction rate is 20%, the total reduction rate is 90%, and the rolling speed is 4m / min;

[0066] (3) Aging treatment is carried out to the primary cold-rolled aluminum alloy strip in...

Embodiment 3

[0080] Embodiment 3: the preparation of Ti-6Al-4V alloy strip

[0081] (1) Use electric pulses to perform rapid solution and water spray cooling and quenching treatment on the hot-rolled Ti-6Al-4V (Ti-5.8wt%Al-4.1wt%V) alloy strip, so that the precipitated phase in the alloy is solid-dissolved in a titanium matrix. The parameters of the electric pulse input to the energized region of the titanium alloy strip blank are: frequency 2500Hz, pulse width 100μs, current density amplitude 5500A / mm 2 , effective current density 900A / mm 2 , the maximum heating temperature is 960°C, the heating time is 30s; the cooling water flow rate of spray water is 80L / min.

[0082] (2) Carry out a cold rolling to the titanium alloy strip material of the electric pulse solution treatment in the step (1), the pass reduction rate is 20%, the total reduction rate is 50%, and the rolling speed is 3m / min;

[0083] (3) Aging treatment is carried out to the primary cold-rolled titanium alloy strip in ste...

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Abstract

The invention discloses a method for strengthening and toughening non-ferrous metal materials. Aiming at the problems of easy oxidation, coarse crystal grains, limited improvement of strength and plasticity, and high energy consumption in the traditional heat treatment process of non-ferrous metal materials, the invention proposes the use of electric pulses to Non-ferrous metal materials are subjected to rapid solution treatment, and then formed once, then aging treatment is performed on the alloy formed once, and secondary forming is performed on the alloy after aging treatment, and finally electric pulse-induced recrystallization treatment is performed on the material formed twice. The characteristics of rapid pulse refinement of matrix grains and precipitated phases that hinder grain growth can be obtained to obtain a microstructure with fine, uniform matrix grains and dispersed strengthening phases. Through the synergistic strengthening and toughening effect of fine grains and precipitated phases, high strength and high Tough non-ferrous materials. Compared with the traditional heat treatment process, the strength and elongation after breaking of the non-ferrous metal material prepared by the process of the invention are respectively increased by more than 10% and more than 20%.

Description

technical field [0001] The invention belongs to the technical field of metal materials, and in particular relates to a method for strengthening and toughening non-ferrous metal materials. Background technique [0002] Non-ferrous metal materials have many properties such as good mechanics, electricity, magnetism, heat conduction and heat dissipation, and are widely used in various fields of national economic construction and national defense and military construction. They are important industrial basic raw materials. With the rapid development of modern industry, especially the rapid development of high-tech fields such as aviation, aerospace, new energy, advanced weaponry and equipment, the performance of copper alloys, aluminum alloys, magnesium alloys, titanium alloys, nickel-based alloys and other non-ferrous metals And processing performance put forward higher and higher requirements. Simultaneously improving the strength and plasticity of the alloy and realizing its ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/00C22F3/00C22F1/08C22F1/053C22F1/18
CPCC22F1/002C22F1/053C22F1/08C22F1/183C22F3/00
Inventor 姜雁斌李周王檬肖柱龚深邱文婷陈东陈伟
Owner CENT SOUTH UNIV
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