Quick-setting cement-based capillary crystalline waterproof material and preparation method thereof
A technology of permeable crystallization and quick-setting cement, applied in the field of quick-setting cement-based permeable crystalline waterproof material and its preparation, can solve the problems of damaged concrete structure, slow hydration speed, long water storage time, etc., and achieve high early strength , to ensure the effect of compactness and high mechanical strength
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Embodiment 1
[0023] The preparation method of quick-setting cement-based permeable crystalline waterproof material comprises the following steps:
[0024] S1: Weigh 10% of potassium fluoride, 10% of tetrasodium aminotrimethylene phosphonate, 20% of sodium phosphate, 10% of sodium oxalate, 10% of magnesium sulfate, and make up the balance with sodium silicate, mix well and grind thoroughly After that, the active masterbatch is obtained;
[0025] S2: After mixing and fully grinding calcium formate, calcium nitrite, sodium metasilicate pentahydrate, and calcium dodecylbenzenesulfonate, they are evenly mixed with micron-sized expanded slag powder with a particle size of 1-3 μm to obtain crystal nuclei Type early strength agent; described crystal nucleus type early strength agent is 1:0.5 by the mass ratio of calcium formate, calcium nitrite, sodium metasilicate pentahydrate, calcium dodecylbenzenesulfonate, micron-scale expansion slag powder: 0.6:0.3:1.2;
[0026] S3: In parts by mass, 20 pa...
Embodiment 2
[0028] The preparation method of quick-setting cement-based permeable crystalline waterproof material comprises the following steps:
[0029] S1: Weigh 12% of potassium fluoride, 12% of tetrasodium aminotrimethylene phosphonate, 21% of sodium phosphate, 12% of sodium oxalate, 12% of magnesium sulfate according to mass percentage, make up the balance with sodium silicate, mix well and grind thoroughly After that, the active masterbatch is obtained;
[0030] S2: After mixing and fully grinding calcium formate, calcium nitrite, sodium metasilicate pentahydrate, and calcium dodecylbenzenesulfonate, they are evenly mixed with micron-sized expanded slag powder with a particle size of 1-3 μm to obtain crystal nuclei Type early strength agent; the mass ratio of described crystal nucleus type early strength agent by calcium formate, calcium nitrite, sodium metasilicate pentahydrate, calcium dodecylbenzenesulfonate, micron-scale expansion slag powder is 1:0.6: 0.9:0.4:1.6;
[0031] S3...
Embodiment 3
[0033] The preparation method of quick-setting cement-based permeable crystalline waterproof material comprises the following steps:
[0034] S1: Weigh 14% of potassium fluoride, 14% of tetrasodium aminotrimethylene phosphonate, 23% of sodium phosphate, 14% of sodium oxalate, 14% of magnesium sulfate according to mass percentage, make up the balance with sodium silicate, mix well and grind thoroughly After that, the active masterbatch is obtained;
[0035] S2: After mixing and fully grinding calcium formate, calcium nitrite, sodium metasilicate pentahydrate, and calcium dodecylbenzenesulfonate, they are evenly mixed with micron-sized expanded slag powder with a particle size of 1-3 μm to obtain crystal nuclei Type early strength agent; described crystal nucleus type early strength agent is 1:0.7 by the mass ratio of calcium formate, calcium nitrite, sodium metasilicate pentahydrate, calcium dodecylbenzenesulfonate, micron-scale expansion slag powder: 1.2:0.5:2;
[0036] S3: ...
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