Preparation method of alkali metal source
A technology of alkali metal source and alkali metal salt, applied in chemical instruments and methods, metal material coating technology, lighting and heating equipment, etc., can solve the problem of uncontrollable powder particle size consistency, poor mixing uniformity, Problems such as debris, to achieve the effect of improving evaporation consistency, avoiding settlement, and good uniformity
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0027] Dissolve 50g of potassium chromate powder as the raw material of the alkali metal source into deionized water, and obtain high-purity potassium chromate powder after repeated evaporation and crystallization, filtering, cleaning, and drying. , D90 is 10um.
[0028] The high-purity 84g Zr ingot and 16g Al ingot were placed in an arc melting crucible, and arc melting was repeated to obtain a ZrAl alloy ingot, which was initially crushed by a jaw crusher, and then transferred to a high-energy ball mill for ball milling. The D90 was 30um and the purity was 99.91%.
[0029] Select 16g of ball-milled ZrAl alloy powder and 4g of potassium chromate powder, stir with 40ml of tert-butanol evenly, transfer to a planetary gravity mixer for uniform mixing, then transfer to a polytetrafluoroethylene container, and use liquid nitrogen to quickly cool the slurry .
[0030] Transfer the frozen slurry to a vacuum freeze dryer, set the partition temperature to -20° C., adjust the drying p...
Embodiment 2
[0033] Dissolve 50g of cesium chromate powder as an alkali metal source raw material into deionized water, and obtain high-purity cesium chromate powder after repeated evaporation and crystallization, filter the crystal, wash and dry, with a purity of 99.995%, and then transfer to a high-energy mill for ball milling , D90 is 100um.
[0034] Place high-purity 70g Zr ingots, 24.6gV ingots, and 5.4g Fe ingots in arc melting crucibles, and repeat arc melting to obtain ZrVFe alloy ingots, which are initially crushed by a jaw crusher, and then transferred to a high-energy ball mill for ball milling. The D90 is 150um, and the purity 99.95%.
[0035] Select 6g of ball-milled ZrVFe alloy powder and 0.4g of cesium chromate powder, stir with 8ml of tert-butanol evenly, transfer to a planetary gravity mixer for uniform mixing, then transfer to a polytetrafluoro container, and use liquid nitrogen to quickly cool the slurry material.
[0036] Transfer the frozen slurry to a vacuum freeze ...
Embodiment 3
[0038] Dissolve 50g of sodium molybdate powder as the raw material of the alkali metal source into deionized water, and obtain high-purity sodium molybdate powder after repeated evaporation and crystallization, filtering crystals, cleaning, and drying, with a purity of 99.99%, and then transfer the ball to a high-energy mill for ball milling , D90 is 1um.
[0039] Place high-purity 15gTi ingots, 45gZr ingots, and 40gV ingots in arc melting crucibles, and repeat arc melting to obtain TiZrV alloy ingots, which are initially crushed by jaw crushers, and then transferred to high-energy ball mills for ball milling. D90 is 10um, and the purity is 99.9%. .
[0040] Select 10g of ball-milled TiZrV alloy powder and 5g of sodium molybdate powder, stir with 18ml of tert-butanol evenly, transfer to a planetary gravity mixer for uniform mixing, then transfer to a polytetrafluoroethylene container, and use dry ice to quickly cool the slurry.
[0041] Transfer the frozen slurry to a vacuum ...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More