Medical soft PVC material suitable for electron beam irradiation sterilization and preparation method thereof
A technology of PVC material and electron beam irradiation, which is applied in the field of modification of medical PVC materials, can solve the problems of mechanical property decline, yellowing of medical PVC materials, etc., and achieve the effect of easy absorption, preventing PVC degradation, and improving stability
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Embodiment 1
[0028] The material provided by the invention is formulated by weight ratio from the following raw materials:
[0029] Medical PVC resin powder: 100 parts;
[0030] Plasticizer DEHP: 40 parts;
[0031] Ultrafine calcium / zinc stabilizer: 1.5 parts;
[0032] Auxiliary heat stabilizer: 12 parts;
[0033] Antioxidant 2246S: 0.25 parts;
[0034] Antioxidant DSTP: 0.25 parts;
[0035] Lubricant: 1.0 parts.
[0036] The ultrafine calcium / zinc stabilizer is composed of 30-60% calcium stearate, 5-10% zinc glycerol, 5-10% zinc acetylacetonate, 10-20% stearoylbenzoylmethane , 5-15% of 1,3-diphenylpropanedione-rare earth metal organic complexes and 10-25% of bis(2,4-di-tert-butylphenol) pentaerythritol diphosphite; The auxiliary heat stabilizer is epoxy linseed oil; the lubricant is composed of 40-60% stearic acid and 40-60% polyethylene wax.
[0037] Specific production steps:
[0038] 1) Zinc stearate, zinc glycerol, zinc acetylacetonate, stearyl benzoyl methane, 1,3-diphenylpro...
Embodiment 2
[0043] The material provided by the invention is formulated by weight ratio from the following raw materials:
[0044] Medical PVC resin powder: 100 parts;
[0045] Plasticizer DEHP: 60 parts;
[0046] Ultrafine calcium / zinc stabilizer: 1 part;
[0047] Auxiliary heat stabilizer: 10 parts;
[0048]Antioxidant 2246S: 0.2 parts;
[0049] Antioxidant DLTP: 0.1 parts;
[0050] Lubricant: 0.8 parts.
[0051] The ultrafine calcium / zinc stabilizer is composed of 30-60% calcium stearate, 5-10% zinc glycerol, 5-10% zinc acetylacetonate, 10-20% stearoylbenzoylmethane , 5-15% of 1,3-diphenylpropanedione-rare earth metal organic complexes and 10-25% of bis(2,4-di-tert-butylphenol) pentaerythritol diphosphite; the auxiliary The heat stabilizer is epoxy linseed oil; the lubricant is composed of 40-60% stearic acid and 40-60% polyethylene wax.
[0052] The preparation method is the same as in Example 1.
Embodiment 3
[0054] The material provided by the invention is formulated by weight ratio from the following raw materials:
[0055] Medical PVC resin powder: 100 parts;
[0056] Plasticizer DEHP: 70 parts;
[0057] Ultrafine calcium / zinc stabilizer: 1.2 parts
[0058] Auxiliary heat stabilizer: 8 parts;
[0059] Antioxidant 2246S: 0.1 parts;
[0060] Antioxidant DLTP: 0.1 parts;
[0061] Lubricant: 0.5 parts.
[0062] The ultrafine calcium / zinc stabilizer is composed of 30-60% calcium stearate, 5-10% zinc glycerol, 5-10% zinc acetylacetonate, 10-20% stearoylbenzoylmethane , 5-15% of 1,3-diphenylpropanedione-rare earth metal organic complexes and 10-25% of bis(2,4-di-tert-butylphenol) pentaerythritol diphosphite; The auxiliary heat stabilizer is epoxy linseed oil; the lubricant is composed of 40-60% stearic acid and 40-60% polyethylene wax.
[0063] The preparation method is the same as in Example 1.
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