Processing technology for prolonging service life of thermal barrier coating of gas engine blade
A gas engine and thermal barrier coating technology, which is applied in metal material coating process, coating, fusion spraying, etc., can solve problems such as coating peeling, cracks, thermal barrier coating failure, etc., to delay fracture, increase Large expansion path, to achieve the effect of service life
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Embodiment 1
[0017] A processing technology for improving the service life of a thermal barrier coating of a gas engine blade, the specific technology is as follows:
[0018] 1) According to the mass ratio of 1:4, weigh methyldichlorosilane and dimethyldichlorosilane, use a fractionation device to purify, collect the purified fractions, and control the fraction temperature of methyldichlorosilane to 39°C , the fraction temperature of dimethyldichlorosilane is 69°C, and then according to the mass volume ratio of 1:20g / ml, add benzene and the collected fractions to the container, mix well and stir rapidly at 240r / min, and then add benzene at 60ml / ml Feed ammonia gas into the reaction vessel at a flow rate of 1 min. When the pH value of the solution reaches 7.5, reduce the flow rate of ammonia gas to 35ml / min, continue to stir and react at 100r / min for 2h, filter out the white precipitate under nitrogen protection, and pass the filtrate through The precursor is obtained after vacuum distillat...
Embodiment 2
[0025] A processing technology for improving the service life of a thermal barrier coating of a gas engine blade, the specific technology is as follows:
[0026] 1) According to the mass ratio of 1:6, weigh methyldichlorosilane and dimethyldichlorosilane, use a fractionation device to purify, collect the purified fractions, and control the fraction temperature of methyldichlorosilane to 40°C , the fraction temperature of dimethyldichlorosilane is 70°C, and then according to the mass volume ratio of 1:25g / ml, add benzene and the collected fractions to the container, mix well and stir rapidly at 260r / min, and then add benzene at 65ml / ml Feed ammonia gas into the reaction vessel at a flow rate of 1 min. When the pH value of the solution reaches 8.0, reduce the flow rate of ammonia gas to 40ml / min, continue to stir and react at 130r / min for 2.5h, filter out the white precipitate under the protection of nitrogen gas, and filter the filtrate The precursor is obtained after vacuum di...
Embodiment 3
[0033] A processing technology for improving the service life of a thermal barrier coating of a gas engine blade, the specific technology is as follows:
[0034] 1) According to the mass ratio of 1:8, weigh methyldichlorosilane and dimethyldichlorosilane, use a fractionation device to purify, collect the purified fractions, and control the fraction temperature of methyldichlorosilane to 41°C , the fraction temperature of dimethyldichlorosilane is 71°C, and then according to the mass volume ratio of 1:30g / ml, add benzene and the collected fractions to the container, mix well and stir rapidly at 300r / min, and then add benzene at a rate of 70ml / ml The flow rate of min is passed into the reaction vessel with ammonia gas. When the pH value of the solution reaches 8, reduce the flow rate of ammonia gas to 45ml / min, continue to stir and react at 150r / min for 3h, filter out the white precipitate under the protection of nitrogen gas, and pass the filtrate through The precursor is obtai...
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