Method for concentrating radioactive solution by using carbon-based magnetic nano composite material
A technology of magnetic nano and composite materials, applied in radioactive purification, nanotechnology, nuclear engineering, etc., can solve problems such as long-term environmental hazards, large radioactive waste, and human health risks
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[0035] In the present invention, the preparation method of the carbon-based magnetic nanocomposite preferably includes the following steps: mixing the acidic aqueous solution of iron salt and the acidic aqueous solution of graphene oxide, adjusting the pH value of the obtained dispersion system to 12, and stirring, A carbon-based magnetic nanocomposite material is obtained. In the present invention, the iron salt is preferably FeCl 2 4H 2 O and FeCl 3 ·6H 2 O mixture; the FeCl 2 4H 2 O and FeCl 3 ·6H 2 The mass ratio of O is preferably 1:2. In the present invention, the solvent of the acidic aqueous solution of the iron salt is preferably a mixed solution of dilute hydrochloric acid and water; the mass concentration of the acidic aqueous solution of the iron salt is preferably 7-8 g·L -1 . In the present invention, the solvent of the acidic aqueous solution of graphene oxide is preferably a mixed solution of dilute hydrochloric acid and water; the mass concentration o...
Embodiment 1
[0047] At 80°C, under the protection of nitrogen, 400mL containing 0.8g FeCl 2 4H 2 O and 2.2 g FeCl 2 ·6H 2 Slowly add the acidic aqueous solution of O to 1600 mL of the acidic aqueous solution containing 0.5 g of graphene oxide; at 85 ° C, quickly add ammonia water to adjust the pH to about 12, stir at 850 rpm for 60 min, and cool the resulting system to room temperature; Magnetic separation, the solid phase is washed with deionized water to neutrality, and then washed with absolute ethanol, and the obtained graphene oxide-based magnetic nanocomposite modified with ferric oxide is placed in water for standby;
[0048] Under the conditions of 298K and pH 7, the activity concentration of 30mL was 147Bq L -1 Co-60( 60 Co) solution (Co mass concentration about 10mg L -1 ) diluted 10 times to 300mL, the activity concentration of the diluted radioactive solution C 1 14.7Bq L -1 ; Add 0.06g ferric oxide-modified graphene oxide-based magnetic nanocomposite (M-GO) in the dilut...
Embodiment 2
[0055] Adsorption and desorption studies were carried out at 298K and a pH value of about 7; non-radioactive isotope Mn solution, Sr solution, and Co solution were mixed with M-GO solution respectively to obtain 30mL mixed solution, each of which contained 0.06g M-GO; initial concentration C of Mn, Sr and Co in each mixed solution 0 Designed for 10mg·L -1 , each mixed solution was shaken for 1 min to reach adsorption equilibrium; 10 mL of uniform mixed solution was taken, filtered, and the obtained solution was detected by ICP-OES to obtain the equilibrium concentration C of Mn, Sr and Co e ;
[0056] Then, add 0.06mL of high-concentration Al solution to the remaining 20mL of the homogeneously mixed solution (Mn, Sr or Co); the initial concentration of Al in the mixed solution is C 0 Designed as two groups (Al-1 and Al-2), each 10mg L -1 and 15mg·L -1 ; The mixed solution was shaken for 1 min to reach the desorption equilibrium; after filtration, it was detected by ICP-OES...
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