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A nanoscale calcium carbonate processing device

A nano-scale calcium carbonate and processing device technology, applied in the direction of calcium carbonate/strontium/barium, calcium/strontium/barium compounds, inorganic chemistry, etc., to achieve the effect of reducing time, uniform reaction and sufficient reaction

Active Publication Date: 2022-07-29
YONGFENG GUANGFENG CHEM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0012] In order to overcome the shortcomings of the above-mentioned prior art, the present invention provides a nanoscale calcium carbonate processing device. The bubbling mechanism divides carbon dioxide, so that carbon dioxide bubbles are uniformly generated at the bottom of the reaction vessel, without considering that the diameter of the reaction vessel is too large to cause gas The problem of uneven distribution along the cross section increases the amount of one-time carbonization reaction and improves production efficiency; at the same time, the bubbling mechanism divides carbon dioxide, so that carbon dioxide is evenly distributed in the liquid phase, making the reaction between carbon dioxide and liquid phase more uniform, and improving the carbon dioxide production efficiency. The low absorption rate makes the reaction more sufficient and reduces the time required for the carbonization reaction; the automatic air intake mechanism can automatically inject carbon dioxide according to the pressure change caused by the consumption of carbon dioxide in the reaction vessel, so that the carbon dioxide in the reaction vessel maintains At a certain level, no manual operation is required, which is convenient, fast, time-saving and labor-saving; the ultrasonic waves emitted by the ultrasonic generator cause cavitation inside the medium, and the nonlinear movement of the cavitation bubbles and the local high pressure generated by the collapse of the cavitation bubbles make the system The energy of each point in the interior changes, causing large fluctuations in energy, weakening the force between molecules, enhancing the mass transfer movement and collision opportunities between reactant molecules, and strengthening the mixing of gas, liquid, and solid phases. The chemical mechanism can cause microscopic vibration inside the solution, accelerate molecular diffusion, and strengthen the mass transfer process. Therefore, ultrasonic waves can make the liquid phase in a nearly ideal mixing state, improve the conversion rate of the liquid phase, and can effectively strengthen the carbonization reaction.

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  • A nanoscale calcium carbonate processing device
  • A nanoscale calcium carbonate processing device
  • A nanoscale calcium carbonate processing device

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0074] like Figure 1-11 As shown, a nanoscale calcium carbonate processing device includes a base 1, a support column 2, a reaction vessel 3, a sealing cover 4, a bubbling mechanism 7, a one-way water inlet and a circulation pipe 8, and the base 1 is provided with a support column 2 A reaction vessel 3 is supported on the support column 2, and the reaction vessel 3 is a cylindrical vessel with an upper end opening, and the reaction vessel 3 bottom end is provided with a liquid outlet 6; The upper end opening of the reaction vessel 3 is sealed with a sealing cover 4, and the sealing cover 4 is provided with a liquid inlet 5; a bubbling mechanism 7 is provided in the reaction vessel 3, and the bubbling mechanism 7 can divide the gas to form bubbles; the bubbling mechanism 7 is provided with a one-way water inlet; the outside of the reaction vessel 3 is provided with a circulation Pipe 8, the upper end of the circulation pipe 8 is communicated with the inner upper part of the re...

Embodiment 2

[0081] like Figure 1-11 As shown, the difference from Embodiment 1 is that an automatic air intake mechanism 9 is also included. The automatic air intake mechanism 9 is communicated with the circulation pipe 8. The automatic air intake mechanism 9 can maintain the carbon dioxide concentration in the reaction vessel 3 to a certain amount.

[0082] The automatic air intake mechanism 9 includes a cylinder block 91, an air intake device 92, a third elastic member 93, an intake pipe 10 and an air outlet pipe 94. The cylinder block 91 has a cylindrical cavity 911 with an upper end closed and a lower end open; the air intake device 92 The whole is cylindrical, the air intake 92 has an air intake cavity 921 with an upper end closed at the lower end, and an air intake groove 922 is opened on the upper part of the air intake 92 away from the circulation pipe 8, and the air intake groove 922 communicates with the outside of the air intake 92. A third elastic member 93 is arranged betwee...

Embodiment 3

[0085] like Figure 1-11 As shown, the difference from Example 1 is that an ultrasonic stirrer is also included, and the ultrasonic stirrer is arranged in the middle of the bottom end of the reaction vessel 3 .

[0086] The ultrasonic agitator includes a cylinder 1001, a first piston 1002, a second piston 1003, an ultrasonic generator 1004, a fourth elastic member 1005, an ejector rod 1006 and a button 1007. A cylinder 1001 is provided in the middle of the bottom end of the reaction vessel 3. The upper end surface of 1001 is flush with the bottom end surface of the reaction vessel 3; the upper part of the cylinder 1001 is slidably provided with a first piston 1002, and the upper end surface of the first piston 1002 is in contact with the lower end surface of the second dividing plate 74; the inner and lower part of the cylinder 1001 slides There is a second piston 1003, and the lower end of the second piston 1003 protrudes from the cylinder 1001; an ultrasonic generator 1004 i...

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Abstract

The invention belongs to the field of nanoscale calcium carbonate processing, in particular to a nanoscale calcium carbonate processing device. A nanoscale calcium carbonate processing device includes a base, a support column, a reaction vessel, a sealing cover, a bubbling mechanism, a one-way water inlet and a circulation pipe. The bubbling mechanism divides the carbon dioxide, so that carbon dioxide bubbles are evenly generated at the bottom of the reaction vessel, without considering the problem of uneven distribution of gas along the cross-section due to the large diameter of the reaction vessel, increasing the amount of one-time carbonization reaction and improving production efficiency; At the same time, the bubbling mechanism divides the carbon dioxide, so that the carbon dioxide is evenly distributed in the liquid phase, so that the reaction between the carbon dioxide and the liquid phase is more uniform, the carbon dioxide absorption rate is improved, the reaction is more sufficient, and the time required for the carbonization reaction is reduced.

Description

technical field [0001] The invention belongs to the field of nanoscale calcium carbonate processing, in particular to a nanoscale calcium carbonate processing device. Background technique [0002] In the processing technology of nano-scale calcium carbonate, it is known from the existing production methods that the carbonization methods are divided into: spray carbonization method, tower carbonization method and supergravity carbonization method. [0003] The specific method of the spray carbonization method is as follows: lime is digested with water into a calcium hydroxide suspension, the suspension is adjusted to a certain concentration and temperature, a certain amount of dispersant is added, and then sprayed into the carbonization tower through the spray nozzle, It is in reverse contact with the rising carbon dioxide gas in the tower to generate calcium carbonate particles. The process conditions are: calcium hydroxide emulsion concentration 1.034-1.069 (relative conce...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J10/00C01F11/18
CPCB01J10/002C01F11/181
Inventor 聂国玶聂雨
Owner YONGFENG GUANGFENG CHEM CO LTD