Phosphorus-containing desulfurized gypsum recycling treatment method
A technology of desulfurization gypsum and treatment method, which is applied in the direction of chemical instruments and methods, single crystal growth, polycrystalline material growth, etc. It can solve the problems that desulfurization gypsum cannot perform well, restricts the application of engineering raw materials, and has a dark yellow color. Achieve the effect of realizing sustainable development, promoting development, and simple methods
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Embodiment 1
[0030] 2. A method for reusing phosphorus-containing desulfurized gypsum, comprising a method for removing impurities from phosphorus-containing desulfurized gypsum and a method for preparing calcium sulfate hemihydrate whiskers;
[0031] The method for removing impurities from phosphorus-containing desulfurized gypsum comprises the following steps:
[0032] S1, the phosphorus-containing detached gypsum is dried in an oven and crushed into powder,
[0033] S2. Configure 100ml of 3mol / L hydrochloric acid solution in a beaker, place it in an oil bath at 95°C and stir for 5 minutes, then add 10g of phosphorus-containing desulfurized gypsum, add 80ml of 0.9mol / L sodium sulfate solution dropwise, and wait for the solution in the beaker to heat up After reaching 95°C, stir for 3 hours, filter the solution after the reaction, and place the filtrate at room temperature to cool until calcium sulfate dihydrate whiskers are precipitated;
[0034] S3. Filter the solution again to obtain ...
Embodiment 2
[0041] A method for reusing phosphorus-containing desulfurized gypsum, including a method for removing impurities from phosphorus-containing desulfurized gypsum and a method for preparing calcium sulfate hemihydrate whiskers;
[0042] Wherein said phosphorus-containing desulfurization gypsum impurity removal method comprises the following steps:
[0043] S1, the phosphorus-containing detached gypsum is dried in an oven and crushed into powder,
[0044] S2. Configure 120ml of 2.5mol / L hydrochloric acid solution in a beaker, place it in an oil bath at 98°C and stir for 5 minutes, then add 10g of phosphorus-containing desulfurized gypsum, add 75ml of 1mol / L sodium sulfate solution dropwise, and wait for the solution in the beaker to heat up Stir for 3.5 hours after reaching 98°C, filter the solution after the reaction, and place the filtrate at room temperature to cool until calcium sulfate dihydrate whiskers are precipitated;
[0045] S3. Filter the solution again to obtain cal...
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