Anti-fog coating and preparation method thereof

An anti-fog coating and graphene technology, applied in the field of coatings, can solve the problems of unsatisfactory perspective effect of anti-fog coatings and comprehensive effects of mechanical properties, achieve good visual perception, improve hardness and wear resistance, and prevent fog droplets. effect

Inactive Publication Date: 2021-06-25
SHENZHEN GRAPHENE LAND LEGEND TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The object of the present invention is to provide an anti-fog coating and its preparation method, aiming to solve the problem of unsatisfactory comprehensive effect of the perspective effect and mechanical properties of the existing anti-fog coating

Method used

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  • Anti-fog coating and preparation method thereof
  • Anti-fog coating and preparation method thereof

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preparation example Construction

[0027] The saturated fatty acid saponification solution may be a saponification solution of stearic acid, lauric acid and palmitic acid. The specific preparation method includes: saponifying saturated fatty acid and sodium hydroxide at a temperature of 70-90°C to obtain saponified liquid, wherein the amount of sodium hydroxide is 20-30% of the mass of saturated fatty acid.

[0028] Further, the mass ratio of the saturated fatty acid saponification liquid and alkylphenol polyoxyethylene ether sodium sulfate is 2-4:1; The mass ratio of betaine ester is 1-2:1; the mass ratio of the first treatment agent and the second treatment agent is 1-2:1. (The hydrophilic modification of graphene in the above-mentioned ratio range can well achieve the effect of modification and can well avoid excessive waste of material consumption.

[0029] Specifically, the preparation method of this modified graphene comprises:

[0030] T1: Add graphene SE1430 into ethylene glycol solvent, and ultrasoni...

Embodiment 1

[0050] A kind of transparent light curing graphene anti-fog coating, its raw material is as shown in table 1.

[0051] Table 1

[0052] Raw material name Dosage (%) SW-808 resin 69 Modified Graphene SE1430 0.01 BYK-333 leveling agent 0.2 TPO photoinitiator 1 DPGDA 15 Butanol 4.79 Absolute ethanol 10

[0053] The preparation method of this transparent light-cured graphene anti-fog coating comprises the steps:

[0054] S1. Weigh the SW-808 resin and put it into the reaction kettle, open the stirrer in the reaction kettle to stir;

[0055] S2. Add modified graphene SE1430 to the reaction kettle (the modification step includes: adding graphene to ethanol, stirring ultrasonically for 30min at a temperature of 60°C and a rotating speed of 300r / min to obtain graphite with a concentration of 50mg / mL Graphene suspension; Adding to graphene suspension is the first surface treatment agent that graphene weight is 5%, and describe...

Embodiment 2

[0061] A kind of transparent light curing graphene anti-fog coating, its raw material is as shown in table 2.

[0062] Table 2

[0063] Raw material name Dosage (%) SW-808 resin 69 Modified Graphene SE1430 0.02 BYK-333 leveling agent 0.2 TPO photoinitiator 1 DPGDA 15 Butanol 4.78 Absolute ethanol 10

[0064] The preparation method of this transparent light-cured graphene anti-fog coating is identical with embodiment 1.

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Abstract

The invention belongs to the technical field of coatings, and particularly relates to an anti-fog coating and a preparation method thereof. The anti-fog coating comprises the following components in parts by weight: 60-80 parts of cured resin, 10-20 parts of a curing monomer, 0.01-0.05 part of modified graphene, 0.5-1.5 parts of a photoinitiator, 0.1-0.3 part of a leveling agent, and 10-23 parts of a solvent, wherein the modified graphene is graphene treated by a surface treating agent for enhancing mechanical properties. According to the anti-fog coating, modified graphene is introduced on the basis of multi-component copolymerization, and the surfaces of graphene particles are specially coated to prepare a functional coating, so that a good anti-fog self-cleaning function is achieved, and meanwhile, the hardness and the wear resistance of a coating are also remarkably improved.

Description

technical field [0001] The invention belongs to the technical field of coatings, and in particular relates to an anti-fog coating and a preparation method thereof. Background technique [0002] Anti-fog coating is a coating that adheres to the surface of the substrate and prevents fog from being produced. The reason for the fog is that hot air hits a cold object and condenses into small water droplets on its surface. The light produces diffuse reflection on the surface of these small water droplets, which gives people the feeling of fog. The formation of water droplets, anti-fog coatings have super-hydrophilic properties on the surface, which increases the surface tension of water. Water cannot form water droplets on its surface, but a layer of water film, which fundamentally prevents the formation of fog. . [0003] The perspective effect and mechanical properties of the existing anti-fog coatings are not ideal, the timeliness of the anti-fog effect is not long enough, th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D175/14C09D5/16C09D7/62
CPCC09D175/14C09D5/1687C08K9/10C08K9/08C08K9/04C08K3/042
Inventor 孙学栋黄李强
Owner SHENZHEN GRAPHENE LAND LEGEND TECH CO LTD
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