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Production technology of ultrasonic-assisted continuous countercurrent extraction of sapindus-saponin

A technology of sapindus saponin and countercurrent extraction, which is applied to the preparation of sugar derivatives, sugar derivatives, and sugar derivatives, etc., can solve the problems of complex process operation, long time consumption, and high product cost.

Pending Publication Date: 2021-07-06
广州市润研基因科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The present invention proposes a production technology for ultrasonic-assisted, continuous countercurrent extraction of sapindus saponin, the purpose of which is to solve the problem of large solvent consumption, long time-consuming, complex process operation and high product cost in the existing extraction process of sapindus saponin , unstable quality, destruction of heat-sensitive substances, waste of limited resources, etc.

Method used

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  • Production technology of ultrasonic-assisted continuous countercurrent extraction of sapindus-saponin
  • Production technology of ultrasonic-assisted continuous countercurrent extraction of sapindus-saponin

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Remove foreign matter, pedicles, twigs and other impurities from the freshly picked Sapindus fruit, sieve to remove dirt and other dust, rinse (drench) with cold water and clean it; use a suitable stainless steel plate to crush Sapindus fruit to make its surface There are certain cracks and cracks. Turn on the ultrasonic energy converter of the continuous extraction device to generate ultrasonic waves; at the same time turn on the hot water delivery pump, and add hot water that has been preheated to 95°C into the extraction pipeline from the liquid filling port at the other end of the continuous extraction device; Put the fresh fruit into the feeding funnel of the continuous extraction device, turn on the motor of the feeding threaded vortex impeller, and slowly push the sapinberry fruit forward into the extraction pipe; Assisted, continuous countercurrent extraction.

[0023] Control the running speed of the motor of the screw vortex impeller so that the residence tim...

Embodiment 2

[0026] Take the dried fruit of Sapindus chinensis after drying, remove impurities such as twigs and foreign objects, peel off the peel and core with a Sapindus fruit core peeling machine, sieve to remove impurities such as stalks and soil, and set aside. Turn on the ultrasonic energy converter of the continuous extraction device to generate ultrasonic waves; at the same time turn on the hot water delivery pump, and add hot water that has been preheated to 80°C into the extraction pipeline from the liquid filling port at the other end of the continuous extraction device; Dried fruit peels are added to the feeding hopper of the continuous extraction device, and the motor of the feeding threaded vortex impeller is turned on, so that the fruit peels of Sapindus chinensis are slowly pushed forward into the extraction pipeline; the peels of Sapinsia chinensis are contacted with hot water, and ultrasonic-assisted, continuous countercurrent extraction of saponin is carried out .

[00...

Embodiment 3

[0030] Take the dried fruit of Sapindus chinensis after drying, remove impurities such as twigs and foreign objects, peel off the peel and core with a Sapindus fruit core peeling machine, sieve to remove impurities such as stalks and soil, and set aside. Turn on the ultrasonic energy converter of the continuous extraction device to generate ultrasonic waves; at the same time, turn on the hot water delivery pump, and add hot water that has been preheated to 55°C into the extraction pipeline from the liquid filling port at the other end of the continuous extraction device; Dried fruit peels are added to the feeding hopper of the continuous extraction device, and the motor of the feeding threaded vortex impeller is turned on, so that the sapinberry fruit is slowly pushed forward into the extraction pipeline; Continuous countercurrent extraction.

[0031] Control the running speed of the motor of the screw vortex impeller so that the residence time of the fresh Sapindus fruit in t...

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Abstract

The invention discloses a production technology of ultrasonic-assisted continuous countercurrent extraction of sapindus-saponin liquid, belongs to the technical field of medicines, chemical engineering and daily chemicals, relates to efficient and rapid extraction and separation of effective components of Chinese herbal medicine plants, and has remarkable effects in the aspects of time saving, consumption reduction and product quality stabilization. The production technology is characterized by comprising the following steps: pretreatment of soapberry fruits, continuous feeding, solvent extraction and countercurrent extraction of the fruits, preliminary filtration of an extracting solution, horizontal screw centrifugal separation, ultrafiltration membrane filtration, reverse osmosis membrane concentration, and centrifugal spin-drying and discharging of pomace. The extraction solvent comprises water but is not limited to water; the extraction temperature of the soapberry fruits in a continuous extraction device is room temperature to 95 DEG C, and the treatment time is 30-480 minutes; the mass ratio of the fruits to the extraction solvent is 1: (3-20), the ultrasonic frequency is 20000-100000Hz, and the intensity is adjustable.

Description

technical field [0001] The invention belongs to the technical fields of medicine, chemical industry and daily chemical industry, relates to the efficient and rapid extraction and separation of effective components of Chinese herbal medicinal plants, and has remarkable effects in saving time, reducing consumption and stabilizing product quality. [0002] technical background [0003] Sapindus delavayi is a deciduous tree belonging to the family Sapindaceae and the genus Sapindus, and it is distributed in various places south of the Huaihe River in my country. The seeds of the plant can be used for medicine (insect repelling); the seed oil can be used to make hardened oil; the peel can be used as a substitute for soap, which can produce rich foam and has strong detergency. The saponin is an excellent natural surfactant, especially suitable for daily chemicals such as washing of fruits and vegetables, tableware, high-grade silk, pure wool fabrics and baby products, and toothpast...

Claims

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Application Information

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IPC IPC(8): A61K36/77C07J63/00C07H15/256C07H1/08A61K131/00
CPCA61K36/77C07J63/008C07H15/256C07H1/08A61K2236/331A61K2236/51A61K2236/53
Inventor 熊远钦孙拥军
Owner 广州市润研基因科技有限公司
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