PIP intelligent regeneration method
A technology of functional layer and charge generation layer, which is applied in the field of organic photoconductor processing, can solve the problems that the OPC coating process of flexible substrates has not been explored, and the flex resistance of the coating has not been paid attention to, so as to achieve high use and promotion value , Facilitate large-scale promotion and application, and highly targeted effects
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preparation example Construction
[0076] In the above-mentioned process, the preparation method of described CT solution comprises the steps:
[0077] The mixture of binder resin, charge transport material and additives is dissolved according to the solid ratio of 1:1-10 to prepare a charge transport layer material solution.
[0078] The charge transport material is polyethylene resin, acrylic resin, polyamide resin, polycarbonate, polyimide resin, vinyl chloride resin, vinyl acetate resin, phenolic resin, polyacrylamide resin, polyurethane resin, polyvinyl alcohol One or more of acetal resin, polyvinyl alcohol resin, polyurethane resin, polyacrylic resin, polyvinylpyridine resin, and water-soluble polyester resin.
[0079] The binder resin is one or more of polycarbonate resin, acrylic resin, polyacrylonitrile resin, phenolic resin, and copolymerized aromatic hydrocarbon resin.
[0080] The additive is any one or more of acrylates, organosiloxane compounds, fatty ether compounds and aminopropene compounds. ...
Embodiment 1
[0093] The first step is to configure CT stripping solution, CT stripping solution, and UC stripping solution respectively.
[0094] The CT stripping solution is a mixture of tetrahydrofuran 60% and toluene 40%; the CG stripping solution is a mixture of butanone 40% diethylene glycol methyl ether 60%; the UC stripping solution is isopropanol 70% and xylene 30%. of the mixture.
[0095] In the second step, the charge blocking layer material solution, the charge generation layer material solution and the charge transport layer material solution are respectively prepared.
[0096] 2-1. Mix and dissolve 30 g of alcohol-soluble nylon resin (, 400 g of ethanol at 50° C. for 4 hours, and prepare a charge blocking material solution for later use.
[0097] 2-2. Mix 15g of titanyl phthalocyanine, 30g of polyethylene glycol butyral (manufactured by Kuraray, Japan, model 120s), and 800g of toluene, grind for 4 hours, and disperse uniformly by ultrasonic to prepare a charge generation mat...
Embodiment 2
[0102] In addition to the configuration process of the charge transport material solution in step 2-3, N, N'-diphenyl-N, N'-bis(4-methylphenyl)-4,4'-biphenyldiamine was changed to It is 50, 200g polycarbonate resin, except that the final film thickness of the charge transport layer is changed to 16um, everything else is the same as that of embodiment 1.
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