Preparation method and application of asphalt modified material based on activated waste rubber powder
A technology of asphalt modification and waste rubber powder, which is applied to building insulation materials, building components, buildings, etc., and can solve problems such as limited use range, short-term aging of asphalt, and microwave activation power affecting activation degree, etc.
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Embodiment 1
[0029] (1) Preparation of epoxy acrylic acid block polymer
[0030] Weigh 15 parts by weight of epoxy resin and 15 parts by weight of styrene monomer into the reaction kettle, gradually raise the temperature to 85°C under the condition of ball mill stirring, then slowly add 5 parts by weight of acrylic acid monomer dropwise, keep the temperature for 2 hours until the reaction is complete , and then lower the temperature to 20°C to separate the balls to obtain epoxy acrylic acid block polymer;
[0031] (2) Activation of waste rubber powder
[0032] Grind 50 parts by weight of waste rubber powder and 4 parts by weight of nano-zinc oxide in a roller grinder for 1 hour, wherein the fineness of the waste rubber powder is 50 mesh, then put it into 150 parts by weight of formic acid and stir at a low speed until it is evenly mixed, then stir at a low speed The stirring rate is 400r / min, and the stirring time is 20h, then add 5 parts by weight of epoxy acrylic acid block polymer obta...
Embodiment 2
[0036] (1) Preparation of epoxy acrylic acid block polymer
[0037] Weigh 15 parts by weight of epoxy resin and 20 parts by weight of styrene monomer into the reaction kettle, gradually raise the temperature to 90°C under the condition of ball mill stirring, then slowly add 6 parts by weight of acrylic acid monomer dropwise, keep the temperature for 2.5h until the reaction completely, and then lower the temperature to 22°C to separate the balls to obtain epoxy acrylic acid block polymer;
[0038] (2) Activation of waste rubber powder
[0039]Grind 50 parts by weight of waste rubber powder and 5 parts by weight of nano-calcium carbonate in a roller grinder for 1.5 hours, wherein the fineness of the waste rubber powder is 80 mesh, then put it into 160 parts by weight of acetic acid and stir at a low speed until it is evenly mixed. The stirring rate of stirring is 500r / min, and the stirring time is 22h, then add 6 parts by weight of epoxy acrylic acid block polymer obtained by s...
Embodiment 3
[0043] (1) Preparation of epoxy acrylic acid block polymer
[0044] Weigh 17 parts by weight of epoxy resin and 17 parts by weight of styrene monomer into the reaction kettle, gradually raise the temperature to 95°C under the condition of ball mill stirring, then slowly add 7 parts by weight of acrylic acid monomer dropwise, keep the temperature for 2 hours until the reaction is complete , and then lower the temperature to 22°C to separate the balls to obtain epoxy acrylic acid block polymer;
[0045] (2) Activation of waste rubber powder
[0046] Grind 80 parts by weight of waste rubber powder and 4 parts by weight of nano-calcium carbonate in a roller grinder for 1.5 h, wherein the fineness of the waste rubber powder is 100 mesh, then put into 170 parts by weight of xylene and stir at a low speed until uniformly mixed, The stirring speed of low-speed stirring is 600r / min, and stirring time is 24h, then add 7 weight parts by the epoxy acrylic acid block polymer that step (1)...
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