Visible light-assisted Fenton promoter as well as preparation method and application thereof
A co-catalyst and visible light technology, applied in catalyst activation/preparation, chemical instruments and methods, physical/chemical process catalysts, etc.
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Embodiment 1
[0034] A preparation method of a visible light-assisted single Fenton co-catalyst is carried out according to the following steps:
[0035] 7.5mmol Zn(Ac) 2 • 2H 2 O was dissolved in 20ml of ethylenediamine solution to obtain solution A, and 30mmol of TAA was dissolved in 10ml of ethylenediamine solvent to form solution B, and solution B was added dropwise to solution A under magnetic stirring and stirred for 2h to obtain a mixed solution, The mixed solution was transferred into the autoclave, and carried out 180 o C, 24h solvent heat treatment; then wash with ethanol and deionized water, after washing, at 60 o Vacuum drying at C temperature for 12h, take out the dried product and grind to obtain Fenton cocatalyst. Its XRD pattern is as figure 1 shown in ZnS-1.
Embodiment 2
[0037] A preparation method of a visible light-assisted Fenton cocatalyst is carried out according to the following steps:
[0038] 2.25mmol CdCl 2 , 5.25mmol Zn(Ac) 2 • 2H 2 O was dissolved in 20ml of ethylenediamine solution to obtain solution A, and 30mmol of TAA was also dissolved in 10ml of ethylenediamine solvent to form solution B. Under magnetic stirring, solution B was added dropwise to solution A and stirred for 2h to obtain a mixed solution , transfer the mixed solution into the autoclave, carry out 180 o C, 24h of solvent heat treatment to obtain the mixture; wash the mixture with ethanol and deionized water, after washing, at 60 o Vacuum drying at C temperature for 12h, take out the dried product and grind to obtain Fenton cocatalyst. Its XRD pattern is as figure 1 shown in ZCS-2.
Embodiment 3
[0040] A preparation method of a visible light-assisted Fenton cocatalyst is carried out according to the following steps:
[0041] 3.75mmol CdCl 2 , 3.75mmol Zn(Ac) 2 • 2H 2 O was dissolved in 20ml of ethylenediamine solution to obtain solution A, and 30mmol of TAA was also dissolved in 10ml of ethylenediamine solvent to form solution B. Under magnetic stirring, solution B was added dropwise to solution A and stirred for 2h to obtain a mixed solution , transfer the mixed solution into the autoclave, carry out 180 o After C, 24h of solvent heat treatment, the mixture was obtained; the mixture was washed with ethanol and deionized water, and the mixture was washed at 60 o Vacuum drying at C temperature for 12h, take out the dried product and grind to obtain Fenton cocatalyst. Its XRD pattern is as figure 1 shown in ZCS-3.
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