Preparation method of lithium iron phosphate battery positive electrode material
A lithium iron phosphate battery and lithium iron phosphate technology, applied in battery electrodes, secondary batteries, circuits, etc., can solve problems such as unsuitable for high rate charge and discharge, poor conductivity, etc., and achieve high charge and discharge performance and good rate performance Effect
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[0020] In order to make the purpose, technical solutions and advantages of the present invention clearer, the technical solutions in the present invention will be clearly and completely described below in conjunction with the accompanying drawings in the present invention.
[0021] The invention provides a method for preparing a positive electrode material of a lithium iron phosphate battery, comprising the following steps:
[0022] (1) dissolving ferric chloride in ethylene glycol, adding sodium acetate and polyethylene glycol, heating; cooling to obtain ferric oxide; oxidizing ferric oxide to nano ferric oxide particles;
[0023] (2) Ball milling: Mix lithium acetate, nanometer ferric oxide, and ammonium dihydrogen phosphate in a molar ratio of Li:Fe:P=1:1:1 and mix with carbon source for ball milling; the ball milling time is 4-6 hours .
[0024] (3) Synthesis of lithium iron phosphate: under protective gas, the powder in step (2) is sintered, and the carbon-coated lithium...
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