Blue fluorescence carbon quantum dot modified super-hydrophobic material as well as preparation method and application thereof
A technology of carbon quantum dots and blue fluorescence, applied in the field of superhydrophobic materials and their preparation, can solve the problems of mutual combination and less research on synergy, and achieve the effects of excellent superhydrophobic performance, low price and wide source of raw materials
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Embodiment 1
[0038] Step 1, the method for preparing modified layered aluminosilicate is to add 3 g of montmorillonite to deionized water, stir at 80 ° C for 3 h, and then add 0.8 g of modifier (octadecyl trimethyl bromide Ammonium chloride) was dissolved in deionized water, and then the modifier solution was mixed with the layered aluminosilicate solution and stirred for 3 h. Centrifuge to obtain precipitates, dry in an oven, grind and sieve to obtain modified montmorillonite.
[0039] Step 2, the preparation method of blue fluorescent carbon quantum dots by hydrothermal method is as follows: weigh 1 g of citric acid and 1 g of banana peel and dissolve them in 20 mL of deionized water, use ammonia water to adjust the pH of the solution to 7, and place them in a hydrothermal reaction kettle , react at 180°C for 12 h, after cooling to room temperature, centrifuge to separate large particles, freeze and dry the supernatant in vacuum to obtain blue fluorescent carbon quantum dots, and dissolv...
Embodiment 2
[0049] Step 1, the method for preparing modified layered aluminosilicate is to first add 3 g of montmorillonite to deionized water, stir at 80 ° C for 3 h, and then add 0.4 g of modifier (hexadecyl trimethyl Ammonium bromide) was dissolved in deionized water, and then the modifier solution was mixed with the layered aluminosilicate solution and stirred for 3 h. Centrifuge to obtain precipitates, dry in an oven, grind and sieve to obtain modified montmorillonite.
[0050] Step 2, the preparation method of the blue fluorescent carbon quantum dots prepared by the hydrothermal method is to weigh 1g of citric acid and 1g of banana peel and dissolve them in 20 mL of deionized water, adjust the pH of the solution to 7 with ammonia water, and place them in a hydrothermal reaction kettle In the process, react at 180°C for 12 h, cool to room temperature, centrifuge to separate large particles, freeze and dry the supernatant in vacuum to obtain blue fluorescent carbon quantum dots, and d...
Embodiment 3
[0054] Step 1, the method for preparing modified layered aluminosilicate is to first add 3 g of talc to deionized water, stir at 60 ° C for 3 h, and then add 0.35 g of modifier (dodecyl trimethyl bromide Ammonium) was dissolved in deionized water, and then the modifier solution was mixed with the layered aluminosilicate solution and stirred for 3 h. Centrifuge to obtain precipitates, dry in an oven, grind and sieve to obtain modified talc.
[0055] Step 2, the preparation method of the blue fluorescent carbon quantum dots prepared by the hydrothermal method is to weigh 1g of citric acid and 1g of banana peel and dissolve them in 20 mL of deionized water, adjust the pH of the solution to 7 with ammonia water, and place them in a hydrothermal reaction kettle , react at 180°C for 12 h, cool to room temperature, centrifuge and separate large particles, freeze and dry the supernatant in vacuum to obtain blue fluorescent carbon quantum dots, and dissolve carbon quantum dots in deion...
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