Preparation method of sponge with photocatalysis function
A photocatalytic and sponge technology, applied in the field of photocatalytic materials, can solve the problems of enhancing bacterial resistance, human health impact, water pollution, etc., and achieve the effects of easy reuse, low cost, and avoidance of corrosion.
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Embodiment 1
[0022] A method of preparing a sponge having a photocatalytic function, comprising the steps of preparing:
[0023] Sl, melamine sponge in absolute ethanol ultrasonic cleaning 10min, dried and then placed in acetone ultrasonic cleaning 10min, and then dried into the water ultrasonic cleaning 10min, dried, immersed in the sponge mass fraction of 5% cationic acrylamide and stirred at rt for 24h, sponges removed, rinsed with water excess surface cationic acrylamide solution, acrylamide-modified cationized sponge;
[0024] S2, the cationic modified acrylamide sponge immersed in a mass fraction of 0.01% graphene oxide (GO) solution of 10 min, rinsed with water after removal GO remaining on the surface, and dried to give sponge GO assembled surface;
[0025] S3, the surface of the assembled GO sponge immersed in a mass fraction of 0.1% of titanium dioxide dispersion, wherein the average particle diameter of titanium dioxide is 5 nm, and the added amount of tetrabutyl titanate, tetrabuty...
Embodiment 2
[0027] A method of preparing a sponge having a photocatalytic function, comprising the steps of preparing:
[0028] Sl, the urethane sponge in absolute ethanol ultrasonic cleaning 10min, dried and then placed in acetone ultrasonic cleaning 10min, and then dried into the water ultrasonic cleaning 10min, dried, immersed in the sponge mass fraction of 6% of a cationic acrylamide and stirred at rt for 24h, sponges removed, rinsed with water excess surface cationic acrylamide solution, acrylamide-modified cationized sponge;
[0029] S2, the cationic modified acrylamide sponge immersed in the mass fraction of 0.02% of graphene oxide (GO) solution of 10 min, rinsed with water after removal GO remaining on the surface, and dried to give sponge GO assembled surface;
[0030] S3, the surface of the assembled GO sponge immersed in a mass fraction of 2% of titanium dioxide dispersion, wherein the average particle diameter of titanium dioxide is 5 nm, and tetrabutyl tetrabutyl added amount of ...
Embodiment 3
[0032] A method of preparing a sponge having a photocatalytic function, comprising the steps of preparing:
[0033] Sl, polyether sponge in absolute ethanol ultrasonic cleaning 10min, dried and then placed in acetone ultrasonic cleaning 10min, and then dried into the water ultrasonic cleaning 10min, dried, immersed in the sponge mass fraction of 10% cationic acrylamide amide solution was stirred at room temperature for 24h, sponges removed, rinsed with water excess surface cationic acrylamide solution, acrylamide-modified cationized sponge;
[0034] S2, the cationic modified acrylamide sponge immersed in a mass fraction of 0.03% of graphene oxide (GO) solution of 10 min, rinsed with water after removal GO remaining on the surface, and dried to give sponge GO assembled surface;
[0035] S3, the surface of the assembled GO sponge immersed in a mass fraction of 5% of titanium dioxide dispersion, wherein the average particle diameter of titanium dioxide is 5 nm, and tetrabutyl tetrabu...
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