High-conductivity copper paste, preparation method, flexible high-conductivity copper film and application of flexible high-conductivity copper film
A high-conductivity, copper paste technology, applied in the field of preparation, flexible high-conductivity copper film, and high-conductivity copper paste, can solve the problems of anti-oxidation technology that needs to be broken through, copper powder is easily oxidized, affecting product performance, etc., and achieves cost-effective green environmental protection , The effect of uniform film resistance distribution and low cost
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Embodiment 1
[0049] Take 110 parts of cardanol-modified novolac resin, add 5 parts of propylene glycol diethyl ester, perform homogenization treatment (revolution at 1000 rpm, time 3 minutes), defoam, and place in an oven at 40°C for 1 hour to obtain resin blend 1.
[0050] Take 20 parts of the above-mentioned resin blend 1, 13 parts of isobutanolamine and 15 parts of triethanolamine, homogenize, homogeneously revolve at 1000rpm for 2min, add 100 parts of the above-mentioned anti-oxidation copper powder C-1 and 24 parts of ethylene glycol Alcohol monobutyl ether, homogenized, homogeneous revolution 1400rpm, time 2min, to obtain a coarse slurry; the coarse slurry was ground with a three-roll mill, and the roll spacing was adjusted to 50μm, 30μm and 10μm in turn to obtain high-conductivity copper Pulp, denoted as P-1.
[0051] Such as figure 1 as shown, figure 1 It is the physical picture of the highly conductive anti-oxidation copper paste P-1 of the present invention.
Embodiment 2
[0053] Take 20 parts of cardanol-modified novolac resin, 5 parts of isobutanolamine and 5 parts of triethanolamine, homogenize, homogeneous revolution 1000rpm, time 3min, add 100 parts of the above anti-oxidation copper powder C-1 and 25 parts of B Glycol monomethyl ether, homogenize, homogeneous revolution 1400rpm, time 2min, to obtain a coarse slurry; the coarse slurry is then ground with a three-roll mill, and the roll spacing is adjusted to 50μm, 30μm and 10μm in turn to obtain high-conductivity copper Pulp, denoted as P-2.
Embodiment 3
[0055] Take 30 parts of octylphenol-modified novolak resin, add 1.6 parts of propylene glycol dimethyl ester, revolutionize 1000rpm homogenize for 2min, add 10 parts of isobutanolamine and 8 parts of N-methyldiethanolamine, and then revolutionize 1000rpm homogenize for 2min, Add 100 parts of the above anti-oxidation copper powder C-2 and 20 parts of ethylene glycol monomethyl ether, homogenize, homogeneous revolution 1400rpm, time 2min, to obtain a coarse slurry; the coarse slurry is then ground with a three-roll mill, The roll distance was adjusted to 50 μm, 30 μm and 10 μm in turn to obtain a high-conductivity copper paste, which was denoted as P-3.
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