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Novel water filtration self-assembly electrostatic spinning nanofiber membrane and preparation method thereof

A technology of nanofiber membrane and electrospinning, which is applied in the fields of fiber chemical characteristics, textiles and papermaking, conjugated artificial filaments, etc., and can solve the problems of low manufacturing process efficiency and other issues

Inactive Publication Date: 2022-03-04
QINGDAO AGRI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Aiming at the deficiencies of the prior art, the present invention provides a novel self-assembled electrospinning nanofiber membrane for water filtration and its preparation method, which solves the problem of low efficiency of the existing electrospinning nanofiber membrane manufacturing process

Method used

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  • Novel water filtration self-assembly electrostatic spinning nanofiber membrane and preparation method thereof
  • Novel water filtration self-assembly electrostatic spinning nanofiber membrane and preparation method thereof
  • Novel water filtration self-assembly electrostatic spinning nanofiber membrane and preparation method thereof

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Embodiment 1

[0050] The embodiment of the present invention provides a method for preparing a novel self-assembled electrospun nanofiber membrane for water filtration, comprising the following steps:

[0051] S1. Preparation of Enteromorpha polysaccharides

[0052] Put the crude polysaccharide of Enteromorpha enteromorpha into a beaker, and add water into the beaker to dissolve it, then put the solution into the osmometer for osmosis treatment, then put the infiltrated solution into the purification equipment for purification treatment, and then put the solution into into the dryer to obtain pure Enteromorpha polysaccharide;

[0053] S2. Prepare the solution

[0054] Weigh a certain amount of Enteromorpha polysaccharide and dissolve it in 50% (V / V) acetic acid, and configure a solution of Enteromorpha polysaccharide with a concentration of 2% (W / V); weigh a certain amount of chitosan and dissolve it in 50% (V / V) / V) In acetic acid, configure a chitosan solution with a concentration of 2%...

Embodiment 2

[0067] The embodiment of the present invention provides a method for preparing a novel self-assembled electrospun nanofiber membrane for water filtration, comprising the following steps:

[0068] S1. Preparation of Enteromorpha polysaccharides

[0069] Put the crude polysaccharide of Enteromorpha enteromorpha into a beaker, and add water into the beaker to dissolve it, then put the solution into the osmometer for osmosis treatment, then put the infiltrated solution into the purification equipment for purification treatment, and then put the solution into into the dryer to obtain pure Enteromorpha polysaccharide;

[0070] S2. Prepare the solution

[0071] Weigh a certain amount of Enteromorpha polysaccharide and dissolve it in 50% (V / V) acetic acid, and configure a solution of Enteromorpha polysaccharide with a concentration of 2% (W / V); weigh a certain amount of chitosan and dissolve it in 50% (V / V) / V) In acetic acid, configure a chitosan solution with a concentration of 2%...

Embodiment 3

[0084] Such as Figure 1-11 As shown, the embodiment of the present invention provides a novel water filtration self-assembled electrospun nanofiber membrane, and a method for observing the surface morphology of the nanofiber membrane, comprising the following steps:

[0085] Cut the fiber membrane into square pieces with a size of 0.5cm*0.5cm, fix it on the stage with conductive glue, observe the surface morphology of the fiber and the morphology of the scaffold with a field emission scanning electron microscope, and analyze the results by SEM , 5 pictures were randomly selected for each sample, 100 fibers were randomly selected for each picture, and the diameter of nanofibers was counted using ImageJ software. Pure Enteromorpha polysaccharides will not form fibers when electrospun from acetic acid. High solubility in solvents, resulting in reduced viscosity, cannot achieve the high degree of entanglement required for efficient electrospinning; however by adding PVA to the CS...

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Abstract

The invention provides a novel water filtration self-assembly electrostatic spinning nanofiber membrane and a preparation method thereof, and relates to the technical field of nanofiber membranes. The object is to develop and characterize an interlayer nanofiber porous support for available thin film composite (TFC) membranes for water filtration. The preparation method of the electrostatic spinning nanofiber membrane comprises the following steps: S1, preparing enteromorpha polysaccharide; s2, preparing a solution; s3, preparing a CS / EPS mixed solution; s4, preparing a PVA solution; s5, preparing a spinning solution; s6, spinning; and S7, final preparation. By mixing the biological polyelectrolyte with a non-toxic, water-soluble, biocompatible and synthetic polymer such as (PVA), the repulsive force in a charged biopolymer solution can be reduced, and the polyvinyl alcohol has the characteristics of good chemical and thermal stability, large specific surface area, high porosity, multiple internal pores and the like, can increase the contact area with cell tissues and increase the adsorption capacity, and can be used for preparing a high-molecular material. The time for reaching adsorption equilibrium is shortened, and the adsorbent can be biodegraded and cannot cause environmental pollution.

Description

technical field [0001] The invention relates to the technical field of nanofiber membranes, in particular to a novel self-assembled electrostatic spinning nanofiber membrane for water filtration and a preparation method thereof. Background technique [0002] Electrospinning is a process performed at room temperature that allows the production of polymer fibers with diameters in the sub-micron range by applying an external electric field, thereby maintaining the bulk properties of the polymer. Electrospun membranes possess some unique structural features, such as high surface-to-volume ratio and very good mechanical properties, which determine their use in a variety of applications, such as air and liquid filtration, tissue engineering, optical and chemical sensors. [0003] Due to the very different chain conformations, hydrodynamic responses, and repulsive forces in solution between natural polymer polyanions, the efficiency and reproducibility of the electrospinning proces...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D04H1/728D04H1/4382D04H1/4309D01F8/18D01F8/10
CPCD04H1/728D04H1/43825D04H1/43838D04H1/4309D01F8/18D01F8/10
Inventor 李秋管娜黄小丽曲丽华刘聪敏
Owner QINGDAO AGRI UNIV