Monocrystal high-temperature alloy directional solidification growth device and method controlled by multi-mode static magnetic field and application of monocrystal high-temperature alloy directional solidification growth device
A technology of directional solidification and superalloy, which is applied in the direction of single crystal growth, single crystal growth, polycrystalline material growth, etc., can solve the problems of unfavorable influence on mechanical properties, severe microscopic segregation, low cooling capacity, etc., and improve the subsequent service performance , cracks are not easy to produce, and the effect of reducing the content of precipitated phase
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Embodiment 1
[0031] In this embodiment, a single crystal superalloy directional solidification growth device controlled by a multi-mode static magnetic field, see figure 1, including a directional solidification system, a temperature measurement system and a magnetic field generator system; the directional solidification system includes a growth cavity, an insulating layer 3, a heating resistor 4, a crucible 5, a pull rod 15, a servo drawing system 17 and a cooling system; the growth cavity The body is composed of a stainless steel furnace shell 2 cooled by cooling water and an internal heat preservation layer 3. A heating resistor 4 is arranged in the inner cavity of the internal heat preservation layer 3, so that the crucible 5 is arranged in the space area of the growth cavity, and the crucible 5 is heated. The crucible 5 is used to load the molten liquid metal 6 to be solidified; using the directional solidification method of pull-down or upward-leading zone melting, a pull rod 15 is ...
Embodiment 2
[0038] This embodiment is basically the same as Embodiment 1, especially in that:
[0039] In this embodiment, a method for preparing a single crystal Ni-based superalloy by directional solidification, the components of the single-crystal Ni-based superalloy prepared in terms of mass percentages are as follows: C: 0.067wt%, Al: 3.58wt%, Ti: 4.07wt%, Ta: 4.99wt%, Cr: 12.03wt%, Co: 8.94wt%, Mo: 1.84wt%, W: 3.91wt%, and the rest is Ni, using the multi-mode static magnetic field control of this embodiment A single crystal superalloy directional solidification growth device, including the following steps: the pulling rate is 20um / s, in one case, a static magnetic field is applied to the directional solidification device, and then a single crystal alloy is prepared by directional solidification; in another case, no magnetic field is applied prepared single crystal alloys.
[0040] Experimental test analysis:
[0041] For the test of the instantaneous tensile properties of the sing...
Embodiment 3
[0043] This embodiment is basically the same as the above-mentioned embodiment, and the special features are:
[0044] In this embodiment, the single crystal growth interface of the liquid metal 6 to be solidified in the crucible 5 is located in the uniform magnetic field area of a single set of magnets, or near the uniform magnetic field area of the geometric center of a double set of magnets. The single crystal growth interface of the liquid metal 6 to be solidified is placed under a controllable magnetic field, which is suitable for the adjustment of various pulling speeds and temperature gradients and other process parameters for directional solidification.
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