Method for producing clean fuel from whole fraction of coal tar
A clean fuel, full distillate technology, applied in the treatment of hydrocarbon oil, petroleum industry, hydrotreating process, etc., to achieve the effect of improving the conversion rate and the yield of the target product, reducing the dosage, and having strong wear resistance and compression resistance.
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[0068] In some more specific embodiments, the preparation method of the fluidized bed hydrogenation catalyst comprises:
[0069] 1) The commercially available basalt fiber chopped yarn is further chopped to a length of about 5 ~ 10 μ M fiber, spare;
[0070] 2) Drying and crushing the natural sponge to obtain the natural sponge powder;
[0071] 3) Mixing the aluminum hydroxide dry rubber powder with the basalt fiber chopped yarn obtained in step 1) and the natural sponge powder obtained in step 2) evenly, adding the extrusion aid, extruding, forming, drying and roasting to obtain the carrier;
[0072] 4) A mixed liquid is formed by adding a non-ionic surfactant to the aqueous solution of the precursor of the metal active component. The precursor of the metal active component is selected from the water-soluble compound containing group VI B and / or group VIII metal elements, and the metal active component is selected from the metal oxide. Then, the carrier obtained in step 3) is i...
Embodiment 1
[0081] Firstly, 2.1g basalt fiber chopped yarn is chopped to a length of 5 ~ 10 μ Fiber; Then 1.0g natural sponge was dried by air blast. The wind speed of the blower was 3.5m / s, the drying temperature was 40 ℃, and the air blast drying time was 20h. After crushing, the natural sponge powder with particle size of 1000 mesh was obtained; The natural sponge powder and the basalt fiber chopped yarn are fully stirred and mixed with 100g aluminum hydroxide dry rubber powder (60% dry basis) at room temperature. Extrusion aids such as citric acid are added in the mixing process, and the amount is subject to the formation of the carrier; After uniform mixing, the mixture is dried and roasted to obtain the carrier. The drying temperature is 100 ℃, and the drying time is 3 hours; The roasting temperature is 400 ℃, and the roasting time is 10 hours.
[0082] To the prepared tungsten cobalt impregnation solution, the concentration is 35.0g metal (in terms of oxide, the ratio of tungsten to co...
Embodiment 2
[0084] Firstly, 1.8g basalt fiber chopped yarn is chopped to a length of 5 ~ 10 μ Fiber; Then 1.8g natural sponge was dried by air blast. The wind speed of the blower was 5m / s, the drying temperature was 50 ℃, and the air blast drying time was 24h. After crushing, the natural sponge powder with particle size of 1400 mesh was obtained; The natural sponge powder and the basalt fiber chopped yarn are fully stirred and mixed with 100g aluminum hydroxide dry rubber powder (80% dry basis) at room temperature. Extrusion aids such as citric acid are added in the mixing process, and the amount is subject to the formation of the carrier; After uniform mixing, the mixture is dried and roasted to obtain the carrier. The drying temperature is 120 ℃, and the drying time is 4 hours; The roasting temperature is 520 ℃, and the roasting time is 6 hours.
[0085] To the above prepared molybdenum cobalt impregnation solution, the concentration is 40.0g metal (in terms of oxide, molybdenum / cobalt ...
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