Eupatorium adenophorum essential oil microcapsule, preparation method thereof and eupatorium adenophorum essential oil modified viscose fiber textile fabric
A technology of Eupatorium adenophorum and microcapsules, which is applied in the direction of microcapsule preparation, microsphere preparation, essential oil/fragrance, etc., and can solve the problem of low bacteriostasis of Eupatoria adenophorum essential oil microcapsules
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[0025] The present invention also provides a preparation method of the above-mentioned Eupatorium adenophorum essential oil microcapsules, comprising the following steps:
[0026] Dissolving the whey protein isolate to obtain the emulsifier aqueous phase;
[0027] Dissolving the diosgenin diosgenin to obtain the dioschina diosgenin solution;
[0028] mixing the essential oil of Eupatorium adenophorum and a cosolvent to obtain the capsule core oil phase;
[0029] performing the first homogenization of the capsule core oil phase and the emulsifier water phase to obtain a mixed emulsion;
[0030] The mixed emulsion is mixed with the yam polysaccharide solution, subjected to the second homogenization, and dried to obtain Eupatorium adenophorum essential oil microcapsules.
[0031] The invention dissolves the whey protein isolate to obtain the emulsifier water phase.
[0032] In the present invention, the reagent for dissolving the whey protein isolate preferably includes a buff...
Embodiment 1
[0058] Wash and dry the fresh underground tubers of yams, peeled and cut into 1cm 3 small pieces; reflux degreasing with 2.5 times the mass of petroleum ether for 5 hours, then suction filter and dry to obtain the filter residue; add 15 times the mass of deionized water to the filter residue, reflux hot water at 70°C for ultrasonic assisted extraction for 150 minutes, take the extract, and The obtained extract was concentrated under reduced pressure, and then 4 times the volume of absolute ethanol was added to the obtained concentrated solution, and left to stand overnight. After suction filtration, the obtained filter residue was washed 3 times successively with absolute ethanol, ether and acetone, and the obtained solid was in Freeze-dry at -80°C for 10 hours to obtain dioscin.
[0059] Fresh branches and leaves of Eupatorium adenophorum were crushed through a 20-mesh sieve to obtain powder of branches and leaves of Eupatorium adenophorum; then deionized water of 15 times th...
Embodiment 2
[0064] Wash and dry the fresh underground tubers of yams, peeled and cut into 1cm 3 Small piece;
[0065] Reflux and degrease with 2 times the mass of petroleum ether for 6 hours, then suction filter and dry to obtain the filter residue; add 10 times the mass of deionized water to the filter residue, reflux hot water at 60°C for 180 minutes with ultrasonic assisted extraction, take the extract, and extract the obtained extract Concentrate under reduced pressure, then add 4 times the volume of absolute ethanol to the obtained concentrated solution, let it stand overnight, and after suction filtration, wash the obtained filter residue three times with absolute ethanol, ether and acetone successively, and the obtained solid is stored at -80°C Freeze-dry for 10 hours to obtain yam polysaccharide.
[0066] Fresh branches and leaves of Eupatorium adenophorum were crushed through a 20-mesh sieve to obtain powder of branches and leaves of Eupatorium adenophorum; then, deionized water...
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